ArticleAnalytical and bioanalytical chemistry2025
Curing reaction kinetics of paper-based phenolic resin laminates-from laboratory measurements to inline quality control.
Article in Analytical and bioanalytical chemistry, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
We describe a comprehensive analysis of the drying and curing kinetics of resol phenol-formaldehyde (PF) resin utilizing multiple different thermophysical and optical measurement techniques and combinations thereof to gain a comprehensive understanding of the physicochemical processes that take place during large-scale production of paper-based PF laminates. This included thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), Fourier-transform infrared evolved gas analysis (FTIR-EGA), and near-infrared (NIR) spectroscopy. In particular, the tailored integration of TGA with simultaneous near-infrared (NIR) spectroscopy in reflection geometry facilitated the evaluation of NIR spectroscopy's suitability for monitoring the ongoing process. This led to the implementation of an NIR-based real-time measurement setup at an industrial production site for a feasibility assessment. NIR spectroscopy in combination with partial least squares (PLS) regression modeling showed highly promising results highlighting the advantages of NIR spectroscopy as a tool for real-time inline quality control for large-scale production of PF resin laminates.
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