ArticleMethods in molecular biology (Clifton, N.J.)2025
Photolabile Linkers for Solid-Phase Synthesis of Oligosaccharides.
Article in Methods in molecular biology (Clifton, N.J.), 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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3 authors.
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Abstract
Photolabile linkers are chemically very stable and can be cleaved under mild conditions without destructive reactions on target molecules. o-Nitrobenzyl-based linkers are widely used in solid phase synthesis. Recently, our group developed several o-nitrobenzylic-based photolabile resins retaining different modifications at reducing-end of glycans after photocleavage. Here, we described the synthesis of three different o-nitrobenzylic derivatives and the immobilization of linkers on commercial Merrifield resin. Subsequently, detailed procedures of loading determination and photocleavage are presented.
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