ArticleJournal of fluorescence2025
Synthesis, Characterization, and Photoluminescence Properties of Binuclear Co(ll), Ni(ll) and Cu(ll) Schiff Base Complexes with μ -1, 1 Azide Bridges.
Article in Journal of fluorescence, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Three new Co(II) (1), Ni(II) (2), and Cu(II) (3) binuclear complexes with versatile azide bridges and Schiff base derived from 2-hydroxy-1-naphthaldehyde and 2-aminothiophenol have been synthesized. Compounds 1-3 were characterized using various techniques, including microanalysis (CHNS), molar conductance, FTIR, UV-visible, 1H-NMR, mass spec, photoluminescence (PL) spectroscopy, thermogravimetric analysis (TGA-DTG), scanning electron microscopy (SEM) and Energy dispersive X-ray (EDX) techniques. Molar conductance values of the newly synthesized complexes indicate that the complexes are electrolytes in solution. Spectroscopic results suggest that the Schiff base acts as a tridentate ligand, bonding to the metal using imino nitrogen, thiol sulphur, and hydroxy oxygen atoms. Upon the incorporation of the azide pseudohalide, the µ -1, 1 bridge are proposed for all the complexes. Electronic spectra of 1-3 suggest an octahedral environment around the metal ions. Schiff base exhibited fluorescence originating from intra-ligand (
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