ArticleJournal of synchrotron radiation2025
Versatile X-ray reflector extension setup for grazing-incidence experiments at SAXS facilities for liquid surface study.
Article in Journal of synchrotron radiation, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Existing beamlines for in situ grazing-incidence small-angle scattering on liquids are either limited in angular range or incompatible with the large sample-detector distance required for submicrometre resolution. We present a low-cost, easily assembled beam-tilting extension for synchrotron-based ultra-small-angle X-ray scattering (USAXS) facilities, enabling grazing-incidence and transmitted scattering (GIUSAXS, GTUSAXS) studies on liquid surfaces. The setup is compatible with standard USAXS beamlines and requires only ∼0.5 m of additional space at the sample stage. It allows X-ray beam incidence angles of up to ∼0.6° at the liquid surface, equal to twice the angle of incidence on a reflector and below its critical angle of typical materials (e.g. silicon, germanium, etc.), and provides access to a q-range of approximately 0.003-0.5 nm
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