ArticleChemistry (Weinheim an der Bergstrasse, Germany)2025
One-Step Thermo-Mechanochemical Syntheses of Metal Phthalocyanines and Polyphthalocyanines.
Article in Chemistry (Weinheim an der Bergstrasse, Germany), 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.
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Who cites it
4 citing papers in PubMed.
- Eco-Friendly Synthesis of Cobalt Phthalocyanine for High-EfficiencyChemistry (Weinheim an der Bergstrasse, Germany) · 2026Article
- Article
- Mechanochemical SChemSusChem · 2026Article
- Recent Advances in Metal Phthalocyanine for Sensing Applications.Nanomaterials (Basel, Switzerland) · 2026Review
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Abstract
We present a thermo-mechanochemical synthesis of metal phthalocyanines with varying metal centers and building blocks. The reactions were performed using a Retsch Mixer Mill 400 equipped with heating jackets, achieving quantitative yields at 120 °C within 2 h. A systematic screening of reaction parameters, including temperature, reaction time, frequency, and liquid-assisted grinding (LAG), revealed that temperature and time significantly influence the reaction outcome, as well as the use of LAG compared to neat grinding, which further enhances the yield. Powder X-ray diffraction analysis of the obtained metal phthalocyanines confirmed the presence of different polymorphs, suggesting a correlation between reaction conditions and crystallinity. Furthermore, the crystalline cobalt polyphthalocyanine (CoPPc) was successfully synthesized with a yield of >99%.
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