ArticleACS nano2025
Real-Time Monitoring of Thermally Induced Twisting-Untwisting of Noncubic Domains in Au Microcrystallites using X-ray Diffraction Microscopy.
Article in ACS nano, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Au bipyramids hosting body-centered orthorhombic and tetragonal lattices (bc(o,t)) exhibit extraordinary stability at ambient conditions and even under high-temperature/high-pressure conditions. The phases undergo conversion to a conventional face-centered cubic (fcc) lattice only during annealing at 700 °C due to the unlocking of the geometrically induced stresses. The spatial distribution of the phases in the crystallite volume has revealed fcc capped bc(o,t) lattices with two halves of the bipyramid twisted by ∼6° along the length with approximately ± 5% strain. Understanding the spatial distribution and dynamics of these phases at high temperatures can provide detailed information on their thermal stability. Herein, using nanoprobe scanning X-ray diffraction microscopy (SXDM),
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