ArticleCommunications chemistry2025
Three-dimensional atomic-scale characterization of titanium oxyhydroxide nanoparticles by data-driven lattice correlation analysis.
Article in Communications chemistry, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
Metal oxyhydroxides are essential nanomaterials for recent technologies because of their diverse applications, such as catalysis, adsorbents, and precursors of metal oxides. These applications rely on the controlled crystal structures of metal oxyhydroxides formed via hydrolyzed metal monomers' condensation. However, characterizing the atomic-scale structures of the metal oxyhydroxides has still been challenging due to their diverse structural types, nanometer-scale sizes, and beam sensitivity. Here, we developed a data-driven analysis approach for atom-resolved transmission electron microscopy images of titanium oxyhydroxide (metatitanic acid) nanoparticles. Lattice spacings and angles were measured for each of the 1300 nanoparticles with random crystal orientations, providing three-dimensional structural information. Our findings reveal their anatase-like structure with alternating layers of titanium dioxide (TiO
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