Evidence map›Paper›PMID 40246759›Full record

ArticleAnalytical and bioanalytical chemistry2025

Determination of cyclopiazonic acid in food samples by using molecularly imprinted polymers based on magnetic halloysite nanotubes.

Miriam Guadaño-Sánchez, Juan J López, Luis A Serrano, Laura Álvaro-Gómez, Lucas Pérez, Matilde Saura-Múzquiz, Javier L Urraca

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Article in Analytical and bioanalytical chemistry, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

7 authors.

Miriam Guadaño-SánchezDepartment of Analytical Chemistry, Faculty of Chemistry, Universidad Complutense de Madrid, 28040, Madrid, Spain.
Juan J LópezDepartment of Analytical Chemistry, Faculty of Chemistry, Universidad Complutense de Madrid, 28040, Madrid, Spain.
Luis A SerranoDepartment of Analytical Chemistry, Faculty of Chemistry, Universidad Complutense de Madrid, 28040, Madrid, Spain.
Laura Álvaro-GómezLaboratorio de Desarrollo Analítico y Quimiometría (LADAQ), Cátedra de Química Analítica I, Facultad de Bioquímica y Ciencias Biológicas, Universidad Nacional del Litoral, Ciudad Universitaria, 3000, Santa Fe, Argentina.
Lucas PérezDepartment of Materials Physics, Faculty of Physics, Universidad Complutense de Madrid, 28040, Madrid, Spain.
Matilde Saura-MúzquizDepartment of Materials Physics, Faculty of Physics, Universidad Complutense de Madrid, 28040, Madrid, Spain. matsaura@ucm.es.
Javier L UrracaDepartment of Analytical Chemistry, Faculty of Chemistry, Universidad Complutense de Madrid, 28040, Madrid, Spain. jurracar@ucm.es.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

A fast, accurate, and simple method of molecularly imprinted solid-phase extraction from magnetic molecularly imprinted polymers (m-MISPE) has been developed for the determination of cyclopiazonic acid (CPA) in food samples. For the synthesis of the magnetic molecularly imprinted polymers, the core-shell method through microwave irradiation was employed. Firstly, as the core halloysite nanotubes were functionalized with magnetite nanoparticles. Then, the molecular imprinted polymer (MIP) shell was created around the halloysite nanotube cores by microwave induction. In the MIP synthesis for the template molecule, an analogous compound in structure to that of CPA has been used as a surrogate molecule to reduce the costs and toxicity produced by the toxin. Besides, washing and elution m-MISPE steps were optimized to eliminate the interferences. Cross-reactivity of the m-MISPE proposed method has been tested with different mycotoxins to determine the selectivity of the polymer towards CPA (imprinting factor (IF): MIP/NIP

Indexed as

Aluminum SilicatesFood AnalysisFood ContaminationIndolesMagnetite NanoparticlesMolecular ImprintingMolecularly Imprinted PolymersNanotubesClayLimit of DetectionOryzaPolymersSolid Phase ExtractionAluminum SilicatesClaycyclopiazonic acidIndolesMagnetite NanoparticlesMolecularly Imprinted PolymersPolymersCyclopiazonic acidHalloysiteMagnetiteMicrowaveMolecularly imprinted polymersMolecularly imprinted solid-phase extractionRice flour samples

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.