ArticleACS electrochemistry2025
In Situ Characterization of the Oxidation Behavior of Carbonate-Based Electrolytes for Lithium-Ion Batteries by Scanning Electrochemical Microscopy.
Article in ACS electrochemistry, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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12 authors.
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Abstract
Lithium-ion batteries (LIBs) have been widely employed as energy storage devices in portable electronics and electric vehicles. Many processes occurring at the electrode/electrolyte interphases lead to performance degradation over time and yet remain poorly understood. We demonstrate new methods based on scanning electrochemical microscopy (SECM) to characterize LIB electrolyte oxidation, which is a key process occurring at the cathode/electrolyte interphase. Our technique leverages a combination of feedback mode and generation/collection mode SECM to provide an electrochemical reversal technique like commonly used cyclic voltammetry or rotating-ring disk electrode methods but one potentially more easily applicable at shorter time scales. We use our method to probe the oxidation of LIB electrolyte components at nonintercalating electrodes including Pt and glassy carbon. We study the oxidation of a common commercially used electrolyte, 1.2 M LiPF
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