Evidence map›Paper›PMID 40192434›Full record

ArticleChemistry (Weinheim an der Bergstrasse, Germany)2025

Infrared Irradiation-Assisted Green Approach for Pd-Catalyzed Buchwald-Hartwig Amination.

Ambra Maria Fiore, Riccardo Ciciriello, Davide Blasi, Pietro Cotugno, Angela Punzi, Gianluca Maria Farinola

Abstract read
In one paragraph

Article in Chemistry (Weinheim an der Bergstrasse, Germany), 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors.

Ambra Maria FioreDipartimento di Chimica, Università degli Studi di Bari Aldo Moro, Via Edoardo Orabona 4, Bari, 70126, Italy.
Riccardo CicirielloDipartimento di Chimica, Università degli Studi di Bari Aldo Moro, Via Edoardo Orabona 4, Bari, 70126, Italy.
Davide BlasiDipartimento di Chimica, Università degli Studi di Bari Aldo Moro, Via Edoardo Orabona 4, Bari, 70126, Italy.
Pietro CotugnoDipartimento di Chimica, Università degli Studi di Bari Aldo Moro, Via Edoardo Orabona 4, Bari, 70126, Italy.
Angela PunziDipartimento di Chimica, Università degli Studi di Bari Aldo Moro, Via Edoardo Orabona 4, Bari, 70126, Italy.ORCID https://orcid.org/0000-0001-5948-6373
Gianluca Maria FarinolaDipartimento di Chimica, Università degli Studi di Bari Aldo Moro, Via Edoardo Orabona 4, Bari, 70126, Italy.

Funding

INSTM INSTM21BAFARINOLANational Quantum Science and Technology Institute PE_00000023
6 · The paper itself

Abstract

We report a novel and green approach for Pd-catalyzed Buchwald-Hartwig amination, assisted by Infrared (IR) irradiation under quasi-solvent-free conditions, in a nonanhydrous environment, and without the exclusion of air. The C-N coupling reactions, performed with a stoichiometric amount of cyclopentyl methyl ether, proceed with moderate-to-good yields using aryl iodides and bromides bearing both electron-donating and electron-withdrawing groups, along with a variety of secondary and primary amines.

Indexed as

Buchwald–Hartwig aminationC–N bond formationgreen solventsinfrared irradiationquasi‐solvent‐free conditions

Identifiers

PMID40192434
PMCPMC12080305

What OpenQuestion holds

Textmetadata
LicenceCC BY
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Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.