ArticleACS applied nano materials2025
In-Flight Observation and Surface Oxidation Modification of Tin Oxide Nanoparticles for Gas Sensing Applications.
Article in ACS applied nano materials, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. An erratum has been issued. Cited by 1 paper.
What it found
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The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.
The trial behind it
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Who cites it
1 citing paper in PubMed.
- Scalable fabrication of gas sensors via spark-ablation printing of semiconductive metal oxide nanoparticles and heterostructures.Microsystems & nanoengineering · 2026Article
Corrections and comments
- Erratum issued
Authors and funding
10 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
Metal oxide nanoparticles are essential in various applications, and the synthesis through gas-phase generation methods offers a rapid and reliable pathway for nanoparticle production. Yet achieving precise control over their formation remains challenging due to the complex nature of oxidation processes. While bulk oxidation states can be assessed via off-line measurements, the dynamic nature of surface oxidation is more difficult to monitor and optimize in real time. Here, we investigate the surface oxidation state of unsupported tin oxide nanoparticles using an aerosol sample-delivery system and in-flight X-ray photoelectron spectroscopy. This powerful method allows the continuous monitoring of the surface oxidation of the gas-phase generated nanoparticles in real time, avoiding uncertainties associated with postcollection alterations. Tin oxide nanoparticles are widely used in gas sensing and catalytic applications, where the surface oxide layer plays a crucial role in determining their performance. Our findings demonstrate how the surface oxidation state of the free-flying particles can be controlled by adjusting the carrier gas composition, in-flight heating temperature, and particle composition. Specifically, the surface oxides of tin are partially reduced when heated in a slightly reducing atmosphere, and the reduction is further enhanced by forming mixed tin-gold nanoparticles. While previous studies on metal oxide nanoparticles have focused predominantly on bulk properties or off-line analysis, this study employs real-time in-flight X-ray photoelectron spectroscopy to investigate details of the surface oxidation state. Understanding the surface oxidation of metal oxide nanoparticles is essential to optimize processes, such as in-flight coating or subsequent deposition into a protective environment. This approach enables the exploration of direct correlations between generation conditions and surface properties, providing valuable insights into optimizing gas-phase nanoparticle synthesis.
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Registered trials
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