Evidence map›Paper›PMID 40170969›Full record

ArticleJournal of applied crystallography2025

An advanced approach combining solid-state NMR with powder diffraction applied to newly synthesized iso-thio-uronium salts.

Jan Rohlíček, Václav Eigner, Jiří Czernek, Jiří Brus

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Journal of applied crystallography, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

0numbers the graph read from it
0cells of the map it votes in
0citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

4 authors.

Jan RohlíčekDepartment of Structure Analysis Institute of Physics of the Czech Academy of Sciences Na Slovance 2 Prague 18221 Czechia.ORCID https://orcid.org/0000-0001-6913-2667
Václav EignerDepartment of Solid State Chemistry University of Chemistry and Technology, Prague Technicka 5 Prague 6 Prague16628 Czechia.ORCID https://orcid.org/0000-0003-1014-3980
Jiří CzernekInstitute of Macromolecular Chemistry of the Czech Academy of Sciences Heyrovskeho nam. 2 Prague 6 Prague16206 Czechia.ORCID https://orcid.org/0000-0003-1474-1822
Jiří BrusInstitute of Macromolecular Chemistry of the Czech Academy of Sciences Heyrovskeho nam. 2 Prague 6 Prague16206 Czechia.ORCID https://orcid.org/0000-0003-2692-612X

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

The focus here is on the structural study of iso-thio-uronium salts and the application of intermolecular distances obtained by solid-state NMR (ssNMR) in determining crystal structures from powder diffraction data. The synthesis of three new tetra-fluoro-borate salts and two bromide salts of iso-thio-uronium compounds is presented first, followed by structural and spectroscopic studies. The tetra-fluoro-borates were further analysed using advanced ssNMR techniques to obtain a set of intermolecular

Indexed as

iso­thio­uronium saltsNMR crystallograpypowder diffractionstructure determination

Identifiers

PMID40170969
PMCPMC11957416

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.