Evidence map›Paper›PMID 40135520›Full record

ArticleJournal of microscopy2025

Hard X-ray spectromicroscopy of Ni-rich cathodes under in situ liquid heating conditions.

Gea T van de Kerkhof, Carmen Murphy, Shahul H Abdulrahman, Timothy Poon, Chris Hawkins, Mengliu Li, Angela E Goode, Julia E Parker, Manfred E Schuster

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Journal of microscopy, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

9 authors.

Gea T van de KerkhofDiamond Light Source, Harwell Science and Innovation Campus, Didcot, UK.
Carmen MurphyJohnson Matthey Technology Centre, Johnson Matthey, Sonning Common, Reading, UK.
Shahul H AbdulrahmanJohnson Matthey Technology Centre, Johnson Matthey, Sonning Common, Reading, UK.
Timothy PoonDiamond Light Source, Harwell Science and Innovation Campus, Didcot, UK.
Chris HawkinsJohnson Matthey Technology Centre, Johnson Matthey, Sonning Common, Reading, UK.
Mengliu LiJohnson Matthey Technology Centre, Johnson Matthey, Sonning Common, Reading, UK.
Angela E GoodeJohnson Matthey Technology Centre, Johnson Matthey, Sonning Common, Reading, UK.
Julia E ParkerDiamond Light Source, Harwell Science and Innovation Campus, Didcot, UK.
Manfred E SchusterJohnson Matthey Technology Centre, Johnson Matthey, Sonning Common, Reading, UK.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

In situ microscopy involves imaging of samples under real reaction conditions. For electron microscopy, micro-electromechanical systems (MEMS) chips have previously been developed that can hold a liquid or gas inside the vacuum of the electron microscope, with electrical contacts that allow for heating or biasing of the sample. These chips have paved the way for high-resolution imaging of dynamic chemical reactions. Here, we report the use of such MEMS chips in an in-house developed setup for a hard X-ray nanoprobe, applied to Ni-rich cathode materials. We investigate the chemical and structural changes in nickel-rich cathodes upon exposure to electrolyte and under heating conditions using hard X-ray spectromicroscopy. As such, we find marked differences in the behaviour of pure LiNiO

Indexed as

hard X‐ray spectromicroscopyin situ liquid heatingMEMS chipsnanoprobenano‐XANESNi‐rich cathodes

Identifiers

PMID40135520
PMCPMC12166338

What OpenQuestion holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.