Di-Cyclohexene Oxide Bridged by DDSQ: Preparation, Characterization, and Application as Fillers for Cyanate Ester Resin.

Xiaoye Gao, Wencheng Gao, Dingyi Lu, Riwei Xu

Abstract read

In one paragraph

Article in Molecules (Basel, Switzerland), 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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5 · Who and what money

Authors and funding

4 authors.

Xiaoye GaoCollege of Materials Science and Engineering, Beijing University of Chemical Technology, Beijing 100029, China.

Wencheng GaoCollege of Materials Science and Engineering, Beijing University of Chemical Technology, Beijing 100029, China.

Dingyi LuCollege of Materials Science and Engineering, Beijing University of Chemical Technology, Beijing 100029, China.

Riwei XuCollege of Materials Science and Engineering, Beijing University of Chemical Technology, Beijing 100029, China.ORCID 0000-0003-2203-3033

Funding

National Natural Science Foundation of China 51573009

6 · The paper itself

Abstract

In order to improve the dielectric properties of existing thermosetting resins, taking advantage of reactive fillers is a simple and feasible option. In this paper, we synthesized a new double epoxycyclohexane double-decker silsesquioxane (DEDDSQ), in which the structure of aliphatic epoxy resin introduced into DDSQ successfully, and the resulting structure of DEDDESQ is confirmed by Fourier transform infrared (FTIR), nuclear magnetic resonance (NMR) spectroscopy, and mass spectrometry (MS). Cyanate ester resin was selected as the case study for the application of DEDDSQ as reactive fillers. A CE/E51/DEDDSQ nanocomposite was fabricated by incorporating a small proportion of E51 resin and DEDDSQ into cyanate ester resin to enhance its comprehensive properties. X-ray diffraction (XRD) and energy-dispersive spectroscopy (EDS) analyses demonstrated that DEDDSQ dispersed uniformly within the resin matrix. Dynamic mechanical analysis (DMA) demonstrated that the CE/E51/8.0DEDDSQ nanocomposites exhibit excellent thermal properties. The glass transition temperature (

Indexed as

cyanate ester resindielectric propertiesnanocompositesPOSS

Identifiers

PMID40076336

DOI10.3390/molecules30051113

PMCPMC11902247

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