Evidence map›Paper›PMID 39940467›Full record

ArticlePolymers2025

Synthesis and Characterization of PLA/Biochar Bio-Composites Containing Different Biochar Types and Content.

Katerina Papadopoulou, Panagiotis A Klonos, Apostolos Kyritsis, Evangelia Tarani, Konstantinos Chrissafis, Ondrej Mašek, Konstantinos Tsachouridis, Antonios D Anastasiou, Dimitrios N Bikiaris

Abstract read
In one paragraph

Article in Polymers, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 8 papers.

0numbers the graph read from it
0cells of the map it votes in
8citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

8 citing papers in PubMed.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

9 authors.

Katerina PapadopoulouLaboratory of Polymer Chemistry and Technology, Department of Chemistry, Aristotle University of Thessaloniki, 54124 Thessaloniki, Greece.
Panagiotis A KlonosLaboratory of Polymer Chemistry and Technology, Department of Chemistry, Aristotle University of Thessaloniki, 54124 Thessaloniki, Greece.ORCID 0000-0001-7222-612X
Apostolos KyritsisDepartment of Physics, National Technical University of Athens, Zografou Campus, 15780 Athens, Greece.
Evangelia TaraniLaboratory of Advanced Materials and Devices, Department of Physics, Aristotle University of Thessaloniki, GR-54124 Thessaloniki, Greece.ORCID 0000-0002-7838-9947
Konstantinos ChrissafisLaboratory of Advanced Materials and Devices, Department of Physics, Aristotle University of Thessaloniki, GR-54124 Thessaloniki, Greece.
Ondrej MašekUK Biochar Research Centre, School of GeoSciences, University of Edinburgh, Alexander Crum Brown Road, Edinburgh EH9 3FF, UK.
Konstantinos TsachouridisDepartment of Chemical Engineering, University of Manchester, Manchester M1 9PL, UK.
Antonios D AnastasiouDepartment of Chemical Engineering, University of Manchester, Manchester M1 9PL, UK.ORCID 0000-0003-3858-9431
Dimitrios N BikiarisLaboratory of Polymer Chemistry and Technology, Department of Chemistry, Aristotle University of Thessaloniki, 54124 Thessaloniki, Greece.ORCID 0000-0001-8458-4952

Funding

EU 952941
6 · The paper itself

Abstract

A series of poly(lactic acid) (PLA)/biochar (BC) bio-composites filled with low amounts (1-5 wt%) of BC were prepared and characterized. The synthesis involved the in situ ring-opening polymerization (ROP) of lactide in the presence of two different types of BC named SWP550 and SWP700, having been produced by pyrolysis of softwood pellets at two different temperatures, 550 and 700 °C, respectively. The bio-composites were characterized by complementary techniques. The successful synthesis of PLA and PLA/BC bio-composites was directly demonstrated by the formation of new bonds, most probably between PLA and BC. Indirect evidence for that was obtained by the systematic molar mass reduction in the presence of BC. BC was found by transmission electron microscopy (TEM) micrographs to be well dispersed at the nanosize level, indicating that in situ polymerization is a technique quite efficient for producing bio-composites with finely dispersed BC additive. The molecular dynamics mapping is performed here via dielectric spectroscopy, moreover, for the first time in these PLA/BC systems. The strong PLA/BC interactions (due to the grafting) led to a systematic deceleration of segmental mobility (elevation of the

Indexed as

biocharbio-compositesenzymatic hydrolysisin situ polymerizationmechanical propertiespoly(lactic acid)segmental mobilitythermal properties

Identifiers

PMID39940467
PMCPMC11820432

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.