ArticleSmall (Weinheim an der Bergstrasse, Germany)2025
Electrochemical Scanning Microwave Microscopy Reveals Ion Intercalation Dynamics and Maps Active Sites in 2D Catalyst.
Article in Small (Weinheim an der Bergstrasse, Germany), 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.
What it found
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The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.
The trial behind it
Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.
Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.
Who cites it
1 citing paper in PubMed.
- Electrochemical Scanning Microwave Microscopy Reveals Ion Intercalation Dynamics and Maps Active Sites in 2D Catalyst.Small (Weinheim an der Bergstrasse, Germany) · 2025Article
Corrections and comments
PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.
Authors and funding
6 authors.
Funding
Abstract
The accelerated demand for electrochemical energy storage urges the need for new, sustainable, and lightweight materials able to store high energy densities rapidly and efficiently. Development of these functional materials requires specialized techniques that can provide a close insight into the electrochemical properties at the nanoscale. For this reason, the electrochemical scanning microwave microscopy (EC-SMM) enabling local measurement of electrochemical properties with nanometer spatial resolution and sensitivity down to atto-Ampere electrochemical currents is introduced. Its power is demonstrated by studying NiCo-layered double hydroxide flakes, revealing active site locations and providing atomistic insights into the catalytic process. EC-SMM's spatial resolution of 16 ± 1 nm allows detailed analysis of edge effects in this 2D material, including localized electrochemical impedance spectroscopy and cyclic voltammetry. Coupled with advanced numerical modeling of diffusion and migration dynamics at the material interface, the findings elucidate the previously hypothesized processes responsible for localized enhancements in electrochemical activity, while pinpointing essential parameters for tuning the thermodynamics of ion intercalation and optimizing surface adsorption.
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What OpenQuestion holds
Registered trials
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