ArticleJournal of applied crystallography2025
Hydro-static behaviour of highly inert Fomblin and Halocarbon fluids as pressure-transmitting media in high-pressure experiments.
Article in Journal of applied crystallography, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 7 papers.
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Who cites it
7 citing papers in PubMed.
- Article
- Development of eco-friendly activated carbon from olive pits for the adsorption of tartrazine with isotherm kinetic and thermodynamic studies.Scientific reports · 2026Article
- Article
- Optimal ratio or historical convention: the use of methanol-ethanol mixtures as pressure-transmitting mediums.Journal of applied crystallography · 2025Article
- Article
- Protonated decafluorobenzophenone and the decafluorobenzophenone-arsenic pentafluoride adduct.Acta crystallographica. Section C, Structural chemistry · 2025Article
- An extended thermal pressure equation of state for sodium fluoride.Journal of applied crystallography · 2025Article
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Authors and funding
5 authors.
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Abstract
A pressure-transmitting medium (PTM) plays an important role in diamond anvil cell (DAC) experiments as it ensures that the sample is exposed to hydro-static pressure. Although PTMs that are liquids under ambient conditions are the easiest to handle and load, the selection of chemically inert liquid media with established hydro-static properties is limited. To widen the choice of highly inert PTMs for high-pressure experiments, the hydro-static behaviours of Fomblin Z60, Fomblin Z25, Fomblin Y LVAC 06/6 and Halocarbon Oil 11-14 were investigated. The ruby fluorescence method was used to monitor the evolution of pressure gradients across the DAC sample chamber during compression and decompression. Fomblin Z60 and Fomblin Z25 perfluoro-polyethers, which are hydro-static to 1.7 and 1.5 GPa, respectively, exhibited the best hydro-static performance, followed by Halocarbon Oil 11-14 with a limit of 1.2 GPa, whereas the non-hydro-static behaviour of Fomblin Y LVAC 06/6 was observed above only 0.6 GPa.
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