ArticleSmall (Weinheim an der Bergstrasse, Germany)2025
Palladium Nanocubes with {100} Facets for Hydrogen Evolution Reaction: Synthesis, Experiment and Theory.
Article in Small (Weinheim an der Bergstrasse, Germany), 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.
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Who cites it
3 citing papers in PubMed.
- Lateral Size Governs Hydrogen Evolution Reaction Mechanisms and Kinetics of Ultrathin Pd Nanosheets in Acidic and Alkaline Electrolytes.The journal of physical chemistry. C, Nanomaterials and interfaces · 2026Article
- Revealing Catalytic Properties of Palladium/Gold Systems toward Hydrogen Evolution, Oxidation, and Absorption with Scanning Electrochemical Microscopy.ACS catalysis · 2025Article
- Palladium Nanocubes with {100} Facets for Hydrogen Evolution Reaction: Synthesis, Experiment and Theory.Small (Weinheim an der Bergstrasse, Germany) · 2025Article
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Authors and funding
10 authors.
Funding
Abstract
Spatially separated palladium nanocubes (Pd NCs) terminated by {100} facets are synthesized using direct micelles approach. The stepwise seed-mediated growth of Pd NCs is applied for the first time. The resulting Pd NCs are thoroughly characterized by HR-TEM, XPS, Raman, ATR-FTIR, TGA, and STEM-EDX spectroscopies. Some traces of residual stabilizer (polyvinylpyrrolidone, PVP) attached to the vertices of Pd NCs are identified after the necessary separation-washing procedure, however, it is vital to avoid aggregation of the NCs. Pd NCs are subsequently and uniformly loaded on Vulcan carbon (≈20 wt.%) for the electrochemical hydrogen cycling. By post-mortem characterizations, it is revealed that their shape and size remained very stable after all electrochemical experiments. However, a strong effect of the NCs size on their hydrogen interaction is revealed. Hydrogen absorption capacity, measured as the H:Pd ratio, ranges from 0.28 to 0.48, while hydrogen evolution and oxidation reactions (HER and HOR) kinetics decrease from 15.5 to 4.6 mA.mg
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Registered trials
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