Evidence map›Paper›PMID 39861319›Full record

ArticlePolymers2025

Exploring the Effect of Annealing on PLA/Carbon Nanotube Nanocomposites: In Search of Efficient PLA/MWCNT Nanocomposites for Electromagnetic Shielding.

Flávio Urbano da Silva, Carlos Bruno Barreto Luna, Fabiano Santana da Silva, José Vinícius Melo Barreto, Debora Pereira Schmitz, Bluma Guenther Soares, Renate Maria Ramos Wellen, Edcleide Maria Araújo

Abstract read
In one paragraph

Article in Polymers, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors.

Flávio Urbano da SilvaAcademic Unit of Materials Engineering, Federal University of Campina Grande, Av. Aprígio Veloso, 882-Bodocongó, Campina Grande 58429-900, PB, Brazil.ORCID 0000-0002-2259-241X
Carlos Bruno Barreto LunaAcademic Unit of Materials Engineering, Federal University of Campina Grande, Av. Aprígio Veloso, 882-Bodocongó, Campina Grande 58429-900, PB, Brazil.ORCID 0000-0002-2441-7439
Fabiano Santana da SilvaAcademic Unit of Materials Engineering, Federal University of Campina Grande, Av. Aprígio Veloso, 882-Bodocongó, Campina Grande 58429-900, PB, Brazil.
José Vinícius Melo BarretoDepartment of Materials Engineering, Federal University of Paraíba, Cidade Universitária, João Pessoa 58051-900, PB, Brazil.ORCID 0000-0002-9062-1163
Debora Pereira SchmitzDepartment of Metallurgical and Materials Engineering-COPPE, PEMM-COPPE, Federal University of Rio de Janeiro, Rio de Janeiro 21941-972, RJ, Brazil.
Bluma Guenther SoaresDepartment of Metallurgical and Materials Engineering-COPPE, PEMM-COPPE, Federal University of Rio de Janeiro, Rio de Janeiro 21941-972, RJ, Brazil.
Renate Maria Ramos WellenDepartment of Materials Engineering, Federal University of Paraíba, Cidade Universitária, João Pessoa 58051-900, PB, Brazil.ORCID 0000-0002-3565-7366
Edcleide Maria AraújoAcademic Unit of Materials Engineering, Federal University of Campina Grande, Av. Aprígio Veloso, 882-Bodocongó, Campina Grande 58429-900, PB, Brazil.

Funding

CAPES 001CNPq 303426/2021-7CNPq 312014/2020-1CNPq 350025/2023-1CNPq 408779/2022-5
6 · The paper itself

Abstract

In this research, poly(lactic acid) (PLA) nanocomposites with multi-walled carbon nanotubes (MWCNT) were produced by extrusion, injection, and compression molding, focusing on electromagnetic shielding. Various amounts of carbon nanotubes (MWCNTs) were tested in PLA matrix, specifically ranging from 1 to 4 parts per hundred resin (phr). The resulting nanocomposites were analyzed before and after undergoing annealing heat treatment. It was observed that as the MWCNT content increased, the melt flow index of PLA decreased. This reduction indicates that the nanotubes were effectively accommodated into the PLA chain. The PLA/MWCNT (2 phr) formulation presented the greatest balance of properties, with potential for electromagnetic shielding application. Scanning electron microscopy (SEM) demonstrated that incorporating 2 phr of carbon nanotubes in PLA promoted good distribution, favoring high electrical conductivity and electromagnetic shielding between 20-22 dB (8.2-18 GHz), corresponding to approximately 99% attenuation. Furthermore, its properties, such as elastic modulus (3156 MPa), tensile strength (65.1 MPa), hardness (77.8 Shore D), and heat deflection temperature (55.3 °C), increased compared to pure PLA. After annealing, the PLA/MWCNT (2 phr) nanocomposite underwent a molecular reordering, resulting in an increased crystalline fraction, as confirmed by X-ray diffraction (XRD). However, the electrical conductivity maintained the same order of magnitude, while the electromagnetic shielding varied from 19.7 to 20 dB. The results indicate that these nanocomposites are promising for electromagnetic shielding applications and can be manufactured in the molten state.

Indexed as

carbon nanotubeselectromagnetic shieldingextruder processingnanocompositespoly(lactic acid)

Identifiers

PMID39861319
PMCPMC11768199

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.