Electrochemical Controlling of Double Microgel Layer Formation on an Electrode Surface via an Electrosensitive Inclusion Complex.

Kamil Marcisz, Mosayeb Gharakhloo, Damian Jagleniec, Jan Pawlowski, Jan Romanski, Marcin Karbarz

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Article in ACS materials Au, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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6 authors.

Kamil MarciszFaculty of Chemistry, University of Warsaw, 1 Ludwika Pasteura Str., PL 02-093 Warsaw, Poland.ORCID https://orcid.org/0000-0002-5750-3798

Mosayeb GharakhlooFaculty of Chemistry, University of Warsaw, 1 Ludwika Pasteura Str., PL 02-093 Warsaw, Poland.

Damian JagleniecFaculty of Chemistry, University of Warsaw, 1 Ludwika Pasteura Str., PL 02-093 Warsaw, Poland.

Jan PawlowskiFaculty of Physics, University of Warsaw, 5 Ludwika Pasteura St., PL 02-093 Warsaw, Poland.

Jan RomanskiFaculty of Chemistry, University of Warsaw, 1 Ludwika Pasteura Str., PL 02-093 Warsaw, Poland.ORCID https://orcid.org/0000-0002-7675-885X

Marcin KarbarzFaculty of Chemistry, University of Warsaw, 1 Ludwika Pasteura Str., PL 02-093 Warsaw, Poland.ORCID https://orcid.org/0000-0002-7813-0513

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6 · The paper itself

Abstract

In this study, we demonstrate the formation of a self-assembled microgel double layer on an electrode surface, utilizing the ability to form electro-responsive, reversible inclusion complexes between microgels modified with ferrocene and β-cyclodextrin in these systems. The bottom layer was based on microgels containing ferrocene moieties and derivatives of cysteine. The presence of the amino acid derivative enabled the formation of the well-packed monolayer on the gold surface through chemisorption, while ferrocene was responsible for electroactivity. The addition of βCD-modified microgel led to the formation of the second monolayer, ultimately creating the double layer. Our investigation focuses on the electrochemically controlled formation and deformation processes of the double microgel layer.

Identifiers

PMID39802141

DOI10.1021/acsmaterialsau.4c00118

PMCPMC11718541

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