ArticleHeliyon2024
Synthesis of ultra-large diameter graphene oxide flakes from natural flake graphite.
Article in Heliyon, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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12 authors.
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Abstract
Graphene and its derivatives are widely used in various fields due to their unique two-dimensional lamellar structure. This study aims to synthesize ultra-large graphene oxide (GO) sheets from natural flake graphite and investigate the factors influencing their size. Using a two-intercalation method based on the modified Hummers' method, we address the challenge of intercalating large-diameter graphene oxide by employing a secondary intercalation technique. Three different approaches were explored to control the size of the produced GO sheets. The results revealed that the completeness of the expansion graphite structure after initial intercalation significantly influenced the final GO sheet size, with more complete expansion leading to larger sheets. Optimal processing conditions were identified, involving soaking natural flake graphite in a mixed solution (H
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