Evidence map›Paper›PMID 39628889›Full record

ArticleJournal of applied crystallography2024

Improving the reliability of small- and wide-angle X-ray scattering measurements of anisotropic precipitates in metallic alloys using sample rotation.

Thomas Perrin, Gilbert A Chahine, Stéphan Arnaud, Arthur Després, Pierre Heugue, Alexis Deschamps, Frédéric De Geuser

Abstract read
In one paragraph

Article in Journal of applied crystallography, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

7 authors.

Thomas PerrinSIMaP Université Grenoble Alpes, CNRS, Grenoble INP 38000Grenoble France.ORCID https://orcid.org/0009-0008-0099-8479
Gilbert A ChahineSIMaP Université Grenoble Alpes, CNRS, Grenoble INP 38000Grenoble France.ORCID https://orcid.org/0000-0003-2550-2325
Stéphan ArnaudInstitut Néel 25 Avenue des Martyrs 38042Grenoble France.
Arthur DesprésSIMaP Université Grenoble Alpes, CNRS, Grenoble INP 38000Grenoble France.
Pierre HeugueDT/MPE, Safran Transmission Systems, 18 Boulevard Louis Seguin, 92707Colombes, France.ORCID https://orcid.org/0000-0002-2204-9134
Alexis DeschampsSIMaP Université Grenoble Alpes, CNRS, Grenoble INP 38000Grenoble France.ORCID https://orcid.org/0000-0002-6038-9201
Frédéric De GeuserSIMaP Université Grenoble Alpes, CNRS, Grenoble INP 38000Grenoble France.ORCID https://orcid.org/0000-0002-2974-9432

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Nanometric precipitates in metallic alloys often have highly anisotropic shapes. Given the large grain size and non-random texture typical of these alloys, performing small- and wide-angle X-ray scattering (SAXS/WAXS) measurements on such samples for determining their characteristics (typically size and volume fraction) results in highly anisotropic and irreproducible data. Rotations of flat samples during SAXS/WAXS acquisitions are presented here as a solution to these anisotropy issues. Two aluminium alloys containing anisotropic precipitates are used as examples to validate the approach with a -45°/45° angular range. Clear improvements can be seen on the SAXS

Indexed as

anisotropymetallic alloysmethodologyrotationSAXS/WAXSsmall- and wide-angle X-ray scattering

Identifiers

PMID39628889
PMCPMC11611286

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.