ArticleReaction chemistry & engineering2025
Monitoring and controlling zeolite synthesis
Article in Reaction chemistry & engineering, 2025. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.
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Who cites it
3 citing papers in PubMed.
- Electro-assisted control over zeolite crystallization and modification: theory, configuration, and applications.Journal of materials chemistry. A · 2026Review
- Reactor-based approach for achieving high-silica zeolites: a fed-batch strategy.Journal of materials chemistry. A · 2026Article
- Dual organic structure-directing agents in zeolite synthesis: cooperation or competition?Materials horizons · 2025Review
Corrections and comments
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Authors and funding
4 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
Most conventional zeolite synthesis takes place in closed batch autoclaves that cannot be monitored or controlled during the process. Moreover, the study of time-dependent parameters of the synthesis with the conventional "cooling-opening" procedure not only reduces accuracy as a series of reactors (never 100% identical) needs to be started in parallel (and stopped at different times), it is also labor intense. Furthermore, the classic batch concept does not permit the intermediate addition of species without disrupting synthesis and the cooling-reheating effects. In this study, we developed a technique for zeolite synthesis monitoring in one-pot experiments using the sampling feature of fed-batch (FB) reactors. These one-pot syntheses can save time and ingredients instead of performing plenty of classic batch experiments. In addition, we could control and manipulate the zeolite synthesis by using the feeding function of the FB reactor and the intermediate addition of precursors at operational temperatures and pressures. Stannosilicate and zincosilicate syntheses were carried out
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Registered trials
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