Evidence map›Paper›PMID 39599114›Full record

ArticleSensors (Basel, Switzerland)2024

Integration of FTIR Spectroscopy, Volatile Compound Profiling, and Chemometric Techniques for Advanced Geographical and Varietal Analysis of Moroccan Eucalyptus Essential Oils.

Aimen El Orche, Abdennacer El Mrabet, Amal Ait Haj Said, Soumaya Mousannif, Omar Elhamdaoui, Siddique Akber Ansari, Hamad M Alkahtani, Shoeb Anwar Ansari, Ibrahim Sbai El Otmani, Mustapha Bouatia

Abstract read
In one paragraph

Article in Sensors (Basel, Switzerland), 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.

0numbers the graph read from it
0cells of the map it votes in
6citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

6 citing papers in PubMed.

  1. Article
  2. Article
  3. Review
  4. Article
  5. Article
  6. Chemometric classification of red ginger (Journal of advanced pharmaceutical technology & research
    Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

10 authors.

Aimen El OrcheLaboratory of Drugs Sciences, Biomedical Research and Biotechnology, Faculty of Medicine and Pharmacy, Hassan II University of Casablanca, B.P. 9154, Casablanca 20250, Morocco.ORCID 0000-0001-5352-2476
Abdennacer El MrabetLaboratory of Drugs Sciences, Biomedical Research and Biotechnology, Faculty of Medicine and Pharmacy, Hassan II University of Casablanca, B.P. 9154, Casablanca 20250, Morocco.ORCID 0000-0003-0880-3222
Amal Ait Haj SaidLaboratory of Drugs Sciences, Biomedical Research and Biotechnology, Faculty of Medicine and Pharmacy, Hassan II University of Casablanca, B.P. 9154, Casablanca 20250, Morocco.
Soumaya MousannifLaboratory of Analytical Chemistry, Team of Formulation and Quality Control of Health Products, Faculty of Medicine and Pharmacy, Mohammed V University in Rabat, Rabat 10090, Morocco.
Omar ElhamdaouiLaboratory of Analytical Chemistry, Team of Formulation and Quality Control of Health Products, Faculty of Medicine and Pharmacy, Mohammed V University in Rabat, Rabat 10090, Morocco.
Siddique Akber AnsariDepartment of Pharmaceutical Chemistry, College of Pharmacy, King Saud University, P.O. Box 2457, Riyadh 11451, Saudi Arabia.ORCID 0000-0003-3966-2282
Hamad M AlkahtaniDepartment of Pharmaceutical Chemistry, College of Pharmacy, King Saud University, P.O. Box 2457, Riyadh 11451, Saudi Arabia.ORCID 0000-0002-6983-8587
Shoeb Anwar AnsariDepartment of Drug Science and Technology, University of Turin, 10124 Turin, Italy.
Ibrahim Sbai El OtmaniLaboratory of Drugs Sciences, Biomedical Research and Biotechnology, Faculty of Medicine and Pharmacy, Hassan II University of Casablanca, B.P. 9154, Casablanca 20250, Morocco.
Mustapha BouatiaLaboratory of Analytical Chemistry, Team of Formulation and Quality Control of Health Products, Faculty of Medicine and Pharmacy, Mohammed V University in Rabat, Rabat 10090, Morocco.

Funding

King Saud University, Riyadh, Saudi Arabia RSPD2024R930
6 · The paper itself

Abstract

Eucalyptus essential oil is widely valued for its therapeutic properties and extensive commercial applications, with its chemical composition significantly influenced by species variety, geographical origin, and environmental conditions. This study aims to develop a reliable method for identifying the geographical origin and variety of eucalyptus oil samples through the application of advanced analytical techniques combined with chemometric methods. Essential oils from Eucalyptus globulus and Eucalyptus camaldulensis were analyzed using Gas Chromatography-Flame Ionization Detection (GC-FID) and Fourier Transform Infrared (FTIR) Spectroscopy. Chemometric analyses, including Orthogonal Partial Least Squares-Discriminant Analysis (O2PLS-DA) and Hierarchical Cluster Analysis (HCA), were utilized to classify the oils based on their volatile compound profiles. Notably, O2PLS-DA was applied directly to the raw FTIR data without additional spectral processing, showcasing its robustness in handling unprocessed data. For geographical origin determination, the GC-FID model achieved a Correct Classification Rate (CCR) of 100%, with 100% specificity and 100% sensitivity for both calibration and validation sets. FTIR spectroscopy achieved a CCR of 100%, specificity of 100%, and sensitivity of 100% for the calibration set, while the validation set yielded a CCR of 95.83%, specificity of 99.02%, and sensitivity of 94.44%. In contrast, the analysis based on species variety demonstrated 100% accuracy across all metrics CCR, specificity, and sensitivity-for both calibration and validation using both techniques. These findings underscore the effectiveness of volatile and infrared spectroscopy profiling for quality control and authentication, providing robust tools for ensuring the consistency and reliability of eucalyptus essential oils in various industrial and therapeutic applications.

Indexed as

EucalyptusOils, VolatileVolatile Organic CompoundsChemometricsCluster AnalysisDiscriminant AnalysisGeographyLeast-Squares AnalysisMoroccoSpectroscopy, Fourier Transform InfraredOils, VolatileVolatile Organic Compoundschemical composition variationschemometric analyseseucalyptus essential oilFTIR Spectroscopyvolatile compound profiles

Identifiers

PMID39599114
PMCPMC11598628

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.