Evidence map›Paper›PMID 39455619›Full record

ArticleScientific reports2024

Effect of ultrasound on the physicochemical, mechanical and adhesive properties of micro-arc oxidized coatings on Ti13Nb13Zr bio-alloy.

Balbina Makurat-Kasprolewicz, Marcin Wekwejt, Luca Pezzato, Anna Ronowska, Jolanta Krupa, Sławomir Zimowski, Stefan Dzionk, Agnieszka Ossowska

Abstract read
In one paragraph

Article in Scientific reports, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors.

Balbina Makurat-KasprolewiczDepartment of Materials Science and Technology, Gdańsk University of Technology, Gdańsk, 80-233, Poland. balbina.makurat-kasprolewicz@pg.edu.pl.
Marcin WekwejtDepartment of Biomaterials Technology, Gdańsk University of Technology, Gdańsk, 80-233, Poland.
Luca PezzatoInstitute of Condensed Matter Chemistry and Energy Technologies, National Research Council of Italy, Padova, 35127, Italy.
Anna RonowskaDepartment of Laboratory Medicine, Medical University of Gdańsk, Gdańsk, 80-210, Poland.
Jolanta KrupaDepartment of Machine Design and Maintenance, AGH University of Kraków, Kraków, 30-059, Poland.
Sławomir ZimowskiDepartment of Machine Design and Maintenance, AGH University of Kraków, Kraków, 30-059, Poland.
Stefan DzionkDepartment of Manufacturing and Production Engineering, Gdańsk University of Technology, Gdańsk, 80-233, Poland.
Agnieszka OssowskaDepartment of Materials Science and Technology, Gdańsk University of Technology, Gdańsk, 80-233, Poland.

Funding

Narodowe Centrum Nauki UMO 2023/49/N/ST5/03551
6 · The paper itself

Abstract

Implant surgeries are increasingly challenging due to their rising number. Achieving the desired biomaterial surface properties to ensure a strong bond with human tissue is a significant issue. This study investigates the influence of ultrasound (US) during the micro-arc oxidation (MAO) process on Ti13Zr13Nb bio-alloy, an area not previously explored, to enhance titanium alloy coatings' properties for biomedical applications. Porous calcium-phosphate-based coatings were successfully deposited on Ti13Zr13Nb using MAO and ultrasound micro-arc oxidation (UMAO). Various properties such as morphology, chemical composition, topography, wettability, surface free energy, thickness, adhesion to the substrate, as well as mechanical and corrosion characteristics were thoroughly analyzed. Cytocompatibility was assessed using human osteoblasts. Using US during the MAO process increased coating roughness (up to ~ 17%), core height (up to 22%), isotropy (up to 17%), thickness (up to ~ 46%), and hardness (up to ~ 18%), depending on MAO parameters and US mode. Optimal coating performance was achieved at 136 mA, 600 s, and a sinusoidal US setting, resulting in the highest isotropy (~ 79%) and rutile quantity (2.6%), the lowest elastic modulus (~ 57 GPa), and the contact angle of ~ 70°, all of which could have contributed to enhancing osteoblast viability in vitro. This study, for the first time, underscores the importance of using the US during the MAO in tailoring the Ti13Zr13Nb for specific biomedical applications.

Indexed as

AlloysCoated Materials, BiocompatibleOsteoblastsOxidation-ReductionSurface PropertiesCell AdhesionHumansMaterials TestingTitaniumUltrasonic WavesAlloysCoated Materials, BiocompatibleTitaniumAdhesionBiomedical applicationNanoindentationPlasma electrolytic oxidationTitanium alloyUltrasound

Identifiers

PMID39455619
PMCPMC11511822

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.