Evidence map›Paper›PMID 39318462›Full record

ArticleRSC advances2024

Iodine/DMSO-catalyzed oxidative deprotection of

Rakshanda Singhal, Manish K Mehra, Babita Malik, Meenakshi Pilania

Abstract read
In one paragraph

Article in RSC advances, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

4 authors.

Rakshanda SinghalDepartment of Chemistry, Manipal University Jaipur Jaipur (Rajasthan) VPO-Dehmi-Kalan, Off Jaipur-Ajmer Express Way Jaipur Rajasthan 303007 India meenakshi.pilania@jaipur.manipal.edu.
Manish K MehraDepartment of Chemistry, Birla Institute of Technology and Science Pilani Pilani Campus Rajasthan 333031 India.
Babita MalikDepartment of Chemistry, Manipal University Jaipur Jaipur (Rajasthan) VPO-Dehmi-Kalan, Off Jaipur-Ajmer Express Way Jaipur Rajasthan 303007 India meenakshi.pilania@jaipur.manipal.edu.
Meenakshi PilaniaDepartment of Chemistry, Manipal University Jaipur Jaipur (Rajasthan) VPO-Dehmi-Kalan, Off Jaipur-Ajmer Express Way Jaipur Rajasthan 303007 India meenakshi.pilania@jaipur.manipal.edu.ORCID https://orcid.org/0000-0003-2211-2444

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

An oxidative deprotection of tosylhyrdazones has been demonstrated to afford benzoic acids using iodine and DMSO system. This efficient oxidative deprotection protocol offers exceptional functional group toleration under mild reaction conditions without any initiators or bases. Notably, the tosylhydrazone with the heteroaryl ring or with the aryl ring having base-sensitive hydroxyl and ester functional groups smoothly afforded the corresponding benzoic acid analogues under developed conditions. Moreover, this method features short reaction times, high product yields and easy purification by avoiding column-chromatographic purification.

Identifiers

PMID39318462
PMCPMC11421529

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.