Evidence map›Paper›PMID 39246255›Full record

ArticleSmall methods2026

In situ Synchrotron X-ray Metrology Boosted by Automated Data Analysis for Real-time Monitoring of Cathode Calcination.

Ruhil Dongol, Arpan Mukherjee, Jianming Bai, Hubertus J J van Dam, Matthew R Carbone, E Frits Abell, Hui Zhong, Akhil Tayal, Lu Ma, Ozgenur Kahvecioglu and 4 more

Abstract read
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In one paragraph

Article in Small methods, 2026. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

14 authors.

Ruhil DongolDepartment of Materials Design and Innovation, University at Buffalo, Buffalo, NY, 14260, USA.
Arpan MukherjeeDepartment of Materials Design and Innovation, University at Buffalo, Buffalo, NY, 14260, USA.
Jianming BaiEnergy and Photon Science, Brookhaven National Laboratory, Upton, NY, 11973, USA.
Hubertus J J van DamComputational Science Initiative, Brookhaven National Laboratory, Upton, NY, 11973, USA.
Matthew R CarboneComputational Science Initiative, Brookhaven National Laboratory, Upton, NY, 11973, USA.
E Frits AbellMaterialsIN Inc, Buffalo, NY, 14216, USA.
Hui ZhongEnergy and Photon Science, Brookhaven National Laboratory, Upton, NY, 11973, USA.
Akhil TayalEnergy and Photon Science, Brookhaven National Laboratory, Upton, NY, 11973, USA.
Lu MaEnergy and Photon Science, Brookhaven National Laboratory, Upton, NY, 11973, USA.
Ozgenur KahveciogluComputational Science Initiative, Brookhaven National Laboratory, Upton, NY, 11973, USA.
Krzysztof Z PupekComputational Science Initiative, Brookhaven National Laboratory, Upton, NY, 11973, USA.
Deyu LuEnergy and Photon Science, Brookhaven National Laboratory, Upton, NY, 11973, USA.
Krishna RajanDepartment of Materials Design and Innovation, University at Buffalo, Buffalo, NY, 14260, USA.
Feng WangArgonne National Laboratory, Lemont, IL, 60439, USA.ORCID https://orcid.org/0000-0003-4068-9212

Funding

Office of Science FWP-PS-030&DE-SC0012704U.S. Department of EnergyU.S. Department of Energy Office of Energy Efficiency and Renewable Energy Vehicle Technologies Office ContractNo.DE-AC02-06CH11357&DE-SC0012704U.S. National Science Foundation
6 · The paper itself

Abstract

Synchrotron X-ray-based in situ metrology is advantageous for monitoring the synthesis of battery materials, offering high throughput, high spatial and temporal resolution, and chemical sensitivity. However, the rapid generation of massive data poses a challenge to on-site, on-the-fly analysis needed for real-time process monitoring. Here, a weighted lagged cross-correlation (WLCC) similarity approach is presented for automated data analysis, which merges with in situ synchrotron X-ray diffraction metrology to monitor the calcination process of the archetypal nickel-based cathode, LiNiO

Indexed as

cathode calcinationdata‐driven analysisin situ metrologynickel‐based cathodesynchrotron X‐rayweighted lagged cross‐correlation

Identifiers

PMID39246255
PMCPMC12825323

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Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.