Oxidative fluorination with Selectfluor: A convenient procedure for preparing hypervalent iodine(V) fluorides.

Samuel M G Dearman, Xiang Li, Yang Li, Kuldip Singh, Alison M Stuart

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In one paragraph

Article in Beilstein journal of organic chemistry, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

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0citing papers in PubMed

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1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

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2 · The registry

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3 · Its place in the literature

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4 · The record

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5 · Who and what money

Authors and funding

5 authors.

Samuel M G DearmanSchool of Chemistry, University of Leicester, Leicester, LE1 7RH, UK.ORCID https://orcid.org/0009-0003-5421-1647

Xiang LiSchool of Chemical Engineering, Dalian University of Technology, No. 2 Linggong Road, Dalian, 116024, P. R. China.

Yang LiSchool of Chemical Engineering, Dalian University of Technology, No. 2 Linggong Road, Dalian, 116024, P. R. China.ORCID https://orcid.org/0000-0002-5719-9044

Kuldip SinghSchool of Chemistry, University of Leicester, Leicester, LE1 7RH, UK.

Alison M StuartSchool of Chemistry, University of Leicester, Leicester, LE1 7RH, UK.ORCID https://orcid.org/0000-0001-5984-4919

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

The ability to investigate hypervalent iodine(V) fluorides has been limited primarily by their difficult preparation traditionally using harsh fluorinating reagents such as trifluoromethyl hypofluorite and bromine trifluoride. Here, we report a mild and efficient route using Selectfluor to deliver hypervalent iodine(V) fluorides in good isolated yields (72-90%). Stability studies revealed that bicyclic difluoro(aryl)-λ

Indexed as

fluorinationfluorobenziodoxoleshalogen bondinghypervalent iodineSelectfluor

Identifiers

PMID39109295

DOI10.3762/bjoc.20.157

PMCPMC11301045

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.