ArticleNanoscale advances2024
Low-cost one-pot synthesis of hydrophobic and hydrophilic monodispersed iron oxide nanoparticles.
Article in Nanoscale advances, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.
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Abstract
The synthesis of Superparamagnetic Iron Oxide Nanoparticles (SPIONs) with size and shape tunability, which is also industrially scalable, remains challenging. Surface functionalization of the nanoparticles is yet another active research subject. Although a variety of inorganic and organometallic precursors have been tried, which are demanding in terms of both cost and effort, the use of iron hydroxide, a simple and cheap iron precursor, has not been explored in detail for the synthesis of SPIONs following a thermal decomposition route. Here, we outline a simple one-pot thermal decomposition route that avoids separate precursor preparation and purification steps and, consequently, is easily scalable. The method involves the alcoholic hydrolysis of a simple iron salt into iron hydroxide, which, on addition of oleic acid, forms the precursor oleate complex
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