Evidence map›Paper›PMID 39040399›Full record

ArticleHeliyon2024

Simultaneous analysis of pesticides and mycotoxins in primary processed foods: The case of bee pollen.

Maria Antonietta Carrera, José Antonio Martinez Martinez, María Dolores Hernando, Amadeo R Fernández-Alba

Abstract read
In one paragraph

Article in Heliyon, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.

0numbers the graph read from it
0cells of the map it votes in
4citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

4 citing papers in PubMed.

  1. Article
  2. Review
  3. Review
  4. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

4 authors.

Maria Antonietta CarreraDepartment of Desertification and Geo-ecology, Experimental Station of Arid Zones, CSIC, Ctra. Sacramento s/n, La Cañada de San Urbano, 04120, Almería, Spain.
José Antonio Martinez MartinezEuropean Union Reference Laboratory for Pesticide Residues in Fruit & Vegetables Agrifood Campus of International Excellence (ceiA3), Department of Chemistry and Physics, University of Almeria, Ctra. Sacramento s/n, La Cañada de San Urbano, 04120, Almería, Spain.
María Dolores HernandoDepartment of Desertification and Geo-ecology, Experimental Station of Arid Zones, CSIC, Ctra. Sacramento s/n, La Cañada de San Urbano, 04120, Almería, Spain.
Amadeo R Fernández-AlbaEuropean Union Reference Laboratory for Pesticide Residues in Fruit & Vegetables Agrifood Campus of International Excellence (ceiA3), Department of Chemistry and Physics, University of Almeria, Ctra. Sacramento s/n, La Cañada de San Urbano, 04120, Almería, Spain.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Primary Processed Foods are a class of food items that are ready for consumption after minimal processing in the supply chain. These products are ubiquitous in our daily diet, but so far a limited number of studies dealt with the optimization of quality control methods to check their content of contaminants. Among primary processed foods, bee pollen is a nutritionally acclaimed food supplement, whose contamination with pesticides and mycotoxins has been largely proven. For this reason, the present study aimed at optimizing for the first time a comprehensive LC-MS/MS method capable of analyzing 282 pesticides and 8 mycotoxins in bee pollen. To obtain a suitable method, two extraction procedures (QuEChERS and Accelerated Solvent Extraction), as well as different chromatographic gradients and columns, were tested. The optimized methodology, comprehending an extraction based on semi-automated QuEChERS, and an analytical method including inert LC column technology, was validated and applied to a sample set of 34 bee pollens. The analyzed samples collectively showed the presence of 41 pesticides and 1 mycotoxin.

Indexed as

Bee pollenLC-MS/MSMycotoxinsPesticidesPrimary processed foods

Identifiers

PMID39040399
PMCPMC11260969

What OpenQuestion holds

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.