Evidence map›Paper›PMID 38906961›Full record

ArticleScientific reports2024

Isolation, characterization and response surface method optimization of cellulose from hybridized agricultural wastes.

Hauwa A Rasheed, Adekunle A Adeleke, Petrus Nzerem, Adebayo I Olosho, Temitayo S Ogedengbe, Seun Jesuloluwa

Abstract read
In one paragraph

Article in Scientific reports, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.

0numbers the graph read from it
0cells of the map it votes in
4citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

4 citing papers in PubMed.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors.

Hauwa A RasheedDepartment of Industrial Chemistry, Nile University of Nigeria, Plot 681, Cadastral Zone C, Airport Road, Jabi, Abuja Federal Capital Territory, Nigeria. hauwaRM@outlook.com.
Adekunle A AdelekeDepartment of Mechanical Engineering, Nile University of Nigeria, Plot 681, Cadastral Zone C, Airport Road, Jabi, Abuja Federal Capital Territory, Nigeria.
Petrus NzeremDepartment of Petroleum and Gas Engineering, Nile University of Nigeria, Plot 681, Cadastral Zone C, Airport Road, Jabi, Abuja Federal Capital Territory, Nigeria.
Adebayo I OloshoDepartment of Chemistry, African University of Science and Technology, Abuja, Nigeria.
Temitayo S OgedengbeDepartment of Mechanical Engineering, Nile University of Nigeria, Plot 681, Cadastral Zone C, Airport Road, Jabi, Abuja Federal Capital Territory, Nigeria.
Seun JesuloluwaDepartment of Mechanical Engineering, Nile University of Nigeria, Plot 681, Cadastral Zone C, Airport Road, Jabi, Abuja Federal Capital Territory, Nigeria.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

This study explores the utilization of eight readily available agricultural waste varieties in Nigeria-sugarcane bagasse, corn husk, corn cob, wheat husk, melina, acacia, mahogany, and ironwood sawdust-as potential sources of cellulose. Gravimetric analysis was employed to assess the cellulose content of these wastes, following which two selected wastes were combined based on their cellulose content and abundance to serve as the raw material for the extraction process. Response Surface Methodology, including Box-Behnken design, was applied to enhance control over variables, establish an optimal starting point, and determine the most favorable reaction conditions. The cellulose extracted under various conditions was comprehensively examined for content, structure, extent of crystallinity, and morphological properties. Characterization techniques such as X-ray Diffraction, Scanning Electron Microscopy, and Fourier Transform Infrared Spectroscopy were employed for detailed analysis. Compositional analysis revealed sugarcane bagasse and corn cob to possess the highest cellulose content, at 41 ± 0.41% and 40 ± 0.32% respectively, with FTIR analysis confirming relatively low C=C bond intensity in these samples. RSM optimization indicated a potential 46% isolated yield from a hybrid composition of sugarcane bagasse and corn cob at NaOH concentration of 2%, temperature of 45 °C, and 10 ml of 38% H

Indexed as

Agricultural wasteAlkaline treatmentCelluloseHydrogen peroxide bleachingSurface response methodology

Identifiers

PMID38906961
PMCPMC11192890

What OpenQuestion holds

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LicenceCC BY
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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.