ArticleMolecules (Basel, Switzerland)2024
The Liquid Jet Endstation for Hard X-ray Scattering and Spectroscopy at the Linac Coherent Light Source.
Article in Molecules (Basel, Switzerland), 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 6 papers.
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Who cites it
6 citing papers in PubMed.
- Electronic and solvent reorganization in proton-coupled electron transfer captured by ultrafast X-rays.Nature communications · 2026Article
- Multiscale phase nucleation driven by photoinduced polarons in a volume-changing material.Nature materials · 2026Article
- Analysis strategies for time-resolved X-ray solution scattering at high repetition rate XFEL sources.Journal of synchrotron radiation · 2026Article
- Determination of Thiol Protonation States by Sulfur X-ray Spectroscopy in Biological Systems.The journal of physical chemistry letters · 2025Article
- Strain-affected ferroelastic domain walls in RbMnFe charge-transfer materials undergoing collective Jahn-Teller distortion.RSC advances · 2024Article
- Ultrafast Optical Pump-Hard X-Ray Probe Spectroscopy of Transition Metal Complexes in Solution at SLAC.Synchrotron radiation newsArticle
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Authors and funding
20 authors.
Funding
Abstract
The ability to study chemical dynamics on ultrafast timescales has greatly advanced with the introduction of X-ray free electron lasers (XFELs) providing short pulses of intense X-rays tailored to probe atomic structure and electronic configuration. Fully exploiting the full potential of XFELs requires specialized experimental endstations along with the development of techniques and methods to successfully carry out experiments. The liquid jet endstation (LJE) at the Linac Coherent Light Source (LCLS) has been developed to study photochemistry and biochemistry in solution systems using a combination of X-ray solution scattering (XSS), X-ray absorption spectroscopy (XAS), and X-ray emission spectroscopy (XES). The pump-probe setup utilizes an optical laser to excite the sample, which is subsequently probed by a hard X-ray pulse to resolve structural and electronic dynamics at their intrinsic femtosecond timescales. The LJE ensures reliable sample delivery to the X-ray interaction point via various liquid jets, enabling rapid replenishment of thin samples with millimolar concentrations and low sample volumes at the 120 Hz repetition rate of the LCLS beam. This paper provides a detailed description of the LJE design and of the techniques it enables, with an emphasis on the diagnostics required for real-time monitoring of the liquid jet and on the spatiotemporal overlap methods used to optimize the signal. Additionally, various scientific examples are discussed, highlighting the versatility of the LJE.
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Registered trials
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