Evidence map›Paper›PMID 38656773›Full record

ArticleJournal of synchrotron radiation2024

A new experimental setup for combined fast differential scanning calorimetry and X-ray photon correlation spectroscopy.

Alessandro Martinelli, Jacopo Baglioni, Peihao Sun, Francesco Dallari, Eloi Pineda, Yajuan Duan, Tobias Spitzbart-Silberer, Fabian Westermeier, Michael Sprung, Giulio Monaco

Open access · goldAbstract read
In one paragraph

Article in Journal of synchrotron radiation, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
0.6field-weighted citation impact, top 35% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed, 5 citations in OpenAlex.

  1. Article
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

10 authors at 3 institutions in 3 countries.

Alessandro MartinelliUniversity of Padova, Department of Physics and Astronomy `Galileo Galilei', Via F. Marzolo 8, 35131 Padova, Italy.ORCID 0000-0002-4971-9986
Jacopo BaglioniUniversity of Padova, Department of Physics and Astronomy `Galileo Galilei', Via F. Marzolo 8, 35131 Padova, Italy.ORCID 0000-0003-0322-0941
Peihao SunUniversity of Padova, Department of Physics and Astronomy `Galileo Galilei', Via F. Marzolo 8, 35131 Padova, Italy.ORCID 0000-0002-3608-1557
Francesco DallariUniversity of Padova, Department of Physics and Astronomy `Galileo Galilei', Via F. Marzolo 8, 35131 Padova, Italy.ORCID 0000-0003-0171-8084
Eloi PinedaDepartment of Physics, Institute of Energy Technologies, Universitat Politècnica de Catalunya - BarcelonaTech, 08019 Barcelona, Spain.ORCID 0000-0002-1871-3848
Yajuan DuanDepartment of Physics, Institute of Energy Technologies, Universitat Politècnica de Catalunya - BarcelonaTech, 08019 Barcelona, Spain.ORCID 0000-0001-8515-6327
Tobias Spitzbart-SilbererDeutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany.
Fabian WestermeierDeutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany.ORCID 0000-0003-0696-206X
Michael SprungDeutsches Elektronen-Synchrotron DESY, Notkestraße 85, 22607 Hamburg, Germany.
Giulio MonacoUniversity of Padova, Department of Physics and Astronomy `Galileo Galilei', Via F. Marzolo 8, 35131 Padova, Italy.ORCID 0000-0003-2497-6422
University of Padua · ITDeutsches Elektronen-Synchrotron DESY · DEUniversitat Politècnica de Catalunya · ES

Funding

European Research Council 101053167
6 · The paper itself

Abstract

Synchrotron-radiation-based techniques are a powerful tool for the investigation of materials. In particular, the availability of highly brilliant sources has opened the possibility to develop techniques sensitive to dynamics at the atomic scale such as X-ray photon correlation spectroscopy (XPCS). XPCS is particularly relevant in the study of glasses, which have been often investigated at the macroscopic scale by, for example, differential scanning calorimetry. Here, we show how to adapt a Flash calorimeter to combine XPCS and calorimetric scans. This setup paves the way to novel experiments requiring dynamical and thermodynamic information, ranging from the study of the crystallization kinetics to the study of the glass transition in systems that can be vitrified thanks to the high cooling rates reachable with an ultrafast calorimeter.

Indexed as

fast differential scanning calorimetryX-ray photon correlation spectroscopy

Identifiers

PMID38656773
PMCPMC11075717
OpenAlexW4395466060

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.