Evidence map›Paper›PMID 38546794›Full record

ArticleAnalytical and bioanalytical chemistry2024

Towards a reference material for microplastics' number concentration-case study of PET in water using Raman microspectroscopy.

Oliver Jacob, Elżbieta Anna Stefaniak, John Seghers, Rita La Spina, Gabriella F Schirinzi, Konstantinos Chatzipanagis, Andrea Held, Håkan Emteborg, Robert Koeber, Martin Elsner and 1 more

Open access · hybridAbstract read
In one paragraph

Article in Analytical and bioanalytical chemistry, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 8 papers.

0numbers the graph read from it
0cells of the map it votes in
8citing papers in PubMed
2.0field-weighted citation impact, top 15% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

8 citing papers in PubMed, 15 citations in OpenAlex.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

11 authors at 3 institutions in 3 countries.

Oliver Jacob *Institute of Water Chemistry, Chair of Analytical Chemistry and Water Chemistry, Technical University of Munich, Lichtenbergstr. 4, 85748, Garching, Germany.ORCID http://orcid.org/0000-0002-4974-5076
Elżbieta Anna Stefaniak *Joint Research Centre (JRC), European Commission (EC), Geel, Belgium.
John SeghersJoint Research Centre (JRC), European Commission (EC), Geel, Belgium.
Rita La SpinaJoint Research Centre (JRC), European Commission (EC), Geel, Belgium.
Gabriella F SchirinziJoint Research Centre (JRC), European Commission (EC), Ispra, Italy.
Konstantinos ChatzipanagisJoint Research Centre (JRC), European Commission (EC), Geel, Belgium.
Andrea HeldJoint Research Centre (JRC), European Commission (EC), Geel, Belgium.
Håkan EmteborgJoint Research Centre (JRC), European Commission (EC), Geel, Belgium.
Robert KoeberJoint Research Centre (JRC), European Commission (EC), Geel, Belgium.
Martin ElsnerInstitute of Water Chemistry, Chair of Analytical Chemistry and Water Chemistry, Technical University of Munich, Lichtenbergstr. 4, 85748, Garching, Germany.ORCID http://orcid.org/0000-0003-4746-9052
Natalia P IvlevaInstitute of Water Chemistry, Chair of Analytical Chemistry and Water Chemistry, Technical University of Munich, Lichtenbergstr. 4, 85748, Garching, Germany. natalia.ivleva@tum.de.ORCID http://orcid.org/0000-0002-7685-5166
European Commission · BETechnical University of Munich · DEJoint Research Centre · IT

Funding

Bundesministerium für Bildung und Forschung 03F0851B
6 · The paper itself

Abstract

Increasing demand for size-resolved identification and quantification of microplastic particles in drinking water and environmental samples requires the adequate validation of methods and techniques that can be used for this purpose. In turn, the feasibility of such validation depends on the existence of suitable certified reference materials (CRM). A new candidate reference material (RM), consisting of polyethylene terephthalate (PET) particles and a water matrix, has been developed. Here, we examine its suitability with respect to a homogeneous and stable microplastic particle number concentration across its individual units. A measurement series employing tailor-made software for automated counting and analysis of particles (TUM-ParticleTyper 2) coupled with Raman microspectroscopy showed evidence of the candidate RM homogeneity with a relative standard deviation of 12% of PET particle counts involving particle sizes >30 µm. Both the total particle count and the respective sums within distinct size classes were comparable in all selected candidate RM units. We demonstrate the feasibility of production of a reference material that is sufficiently homogeneous and stable with respect to the particle number concentration.

Indexed as

HomogeneityMicroplasticsParticle number concentrationRaman microspectroscopyReference materialStability

Identifiers

PMID38546794
PMCPMC11045626
OpenAlexW4393265650

What OpenQuestion holds

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LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.