Evidence map›Paper›PMID 38536667›Full record

ArticleJournal of the American Chemical Society2024

High Temperature Electron Diffraction on Organic Crystals:

Yaşar Krysiak, Sergi Plana-Ruiz, Lothar Fink, Edith Alig, Ulrich Bahnmüller, Ute Kolb, Martin U Schmidt

Abstract read
In one paragraph

Article in Journal of the American Chemical Society, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.

0numbers the graph read from it
0cells of the map it votes in
3citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

3 citing papers in PubMed.

  1. Article
  2. Reuniting crystallography with real space: Ab initio structure elucidation with 4D-STEM.Proceedings of the National Academy of Sciences of the United States of America · 2025
    Article
  3. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

7 authors.

Yaşar KrysiakInstitute of Inorganic Chemistry, Leibniz University Hannover, Callinstraße 9, 30167 Hannover, Germany.ORCID 0000-0001-9314-8394
Sergi Plana-RuizDepartment of Materials and Geoscience, Technische Universität Darmstadt, Petersenstrasse 23, 64287 Darmstadt, Germany.ORCID 0000-0002-4047-8362
Lothar FinkInstitute of Inorganic and Analytical Chemistry, Goethe University Frankfurt am Main, Max-von-Laue-Str. 7, 60438 Frankfurt am Main, Germany.ORCID 0000-0001-8369-1756
Edith AligInstitute of Inorganic and Analytical Chemistry, Goethe University Frankfurt am Main, Max-von-Laue-Str. 7, 60438 Frankfurt am Main, Germany.
Ulrich BahnmüllerInstitute of Inorganic Chemistry, Leibniz University Hannover, Callinstraße 9, 30167 Hannover, Germany.
Ute KolbDepartment of Materials and Geoscience, Technische Universität Darmstadt, Petersenstrasse 23, 64287 Darmstadt, Germany.
Martin U SchmidtInstitute of Inorganic and Analytical Chemistry, Goethe University Frankfurt am Main, Max-von-Laue-Str. 7, 60438 Frankfurt am Main, Germany.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Small molecule structures and their applications rely on good knowledge of their atomic arrangements. However, the crystal structures of these compounds and materials, which are often composed of fine crystalline domains, cannot be determined with single-crystal X-ray diffraction. Three-dimensional electron diffraction (3D ED) is already becoming a reliable method for the structure analysis of submicrometer-sized organic materials. The reduction of electron beam damage is essential for successful structure determination and often prevents the analysis of organic materials at room temperature, not to mention high temperature studies. In this work, we apply advanced 3D ED methods at different temperatures enabling the accurate structure determination of two phases of Pigment Orange 34 (C

Identifiers

PMID38536667
PMCPMC11009952

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.