Evidence map›Paper›PMID 38497561›Full record

ArticleThe Journal of organic chemistry2024

Microwave-Assisted One-Pot Telescoped Synthesis of 2-Amino-1,3-thiazoles, Selenazoles, Imidazo[1,2-

Pablo Macías-Benítez, Alfonso Sierra-Padilla, Francisco M Guerra, F Javier Moreno-Dorado

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in The Journal of organic chemistry, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Article
  2. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

4 authors.

Pablo Macías-BenítezDepartamento de Química Orgánica e Instituto de Biomoléculas, Facultad de Ciencias, Universidad de Cádiz, Polígono Río San Pedro s/n., 11510 Puerto Real, Cádiz, Spain.
Alfonso Sierra-PadillaDepartamento de Química Orgánica e Instituto de Biomoléculas, Facultad de Ciencias, Universidad de Cádiz, Polígono Río San Pedro s/n., 11510 Puerto Real, Cádiz, Spain.ORCID 0000-0002-7353-7971
Francisco M GuerraDepartamento de Química Orgánica e Instituto de Biomoléculas, Facultad de Ciencias, Universidad de Cádiz, Polígono Río San Pedro s/n., 11510 Puerto Real, Cádiz, Spain.ORCID 0000-0001-8557-0018
F Javier Moreno-DoradoDepartamento de Química Orgánica e Instituto de Biomoléculas, Facultad de Ciencias, Universidad de Cádiz, Polígono Río San Pedro s/n., 11510 Puerto Real, Cádiz, Spain.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Primary and secondary alcohols have been converted into 2-amino-1,3-thiazoles under microwave irradiation, employing trichloroisocyanuric acid (TCCA) as a dual oxidant and chlorine source, TEMPO as a co-oxidant, and thiourea. Secondary alcohols underwent a single-stage, one-pot conversion process, while primary alcohols required a two-stage, one-pot procedure. Both transformations were completed within minutes (25-45 min). The versatility of this protocol extends to the synthesis of other heterocycles, including 1,3-selenazoles, 2-aminoimidazoles, imidazo[1,2-

Identifiers

PMID38497561
PMCPMC12863238

What OpenQuestion holds

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LicenceCC BY
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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.