Evidence map›Paper›PMID 38495385›Full record

ArticleMacromolecules2024

Study of the Crystal Structure and Hydrogen Bonding during Cold Crystallization of Poly(trimethylene 2,5-furandicarboxylate).

Oscar Toledano, Oscar Gálvez, Mikel Sanz, Carlos Garcia Arcos, Esther Rebollar, Aurora Nogales, Mari Cruz García-Gutiérrez, Gonzalo Santoro, Izabela Irska, Sandra Paszkiewicz and 2 more

Abstract read
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In one paragraph

Article in Macromolecules, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

0numbers the graph read from it
0cells of the map it votes in
0citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

12 authors.

Oscar ToledanoCICECO - Aveiro Institute of Materials, Universidade de Aveiro, Aveiro 3810-193, Portugal.ORCID https://orcid.org/0000-0002-8263-807X
Oscar GálvezDepto. Física Interdisciplinar, Universidad Nacional de Educación a Distancia (UNED), Fac. Ciencias Av. de Esparta s/n, 28232 Las Rozas de Madrid, Spain.
Mikel SanzDepto. Física Interdisciplinar, Universidad Nacional de Educación a Distancia (UNED), Fac. Ciencias Av. de Esparta s/n, 28232 Las Rozas de Madrid, Spain.
Carlos Garcia ArcosDepto. Física Interdisciplinar, Universidad Nacional de Educación a Distancia (UNED), Fac. Ciencias Av. de Esparta s/n, 28232 Las Rozas de Madrid, Spain.ORCID https://orcid.org/0000-0003-0632-6901
Esther RebollarInstituto de Química Física Blas Cabrera, IQF-CSIC, Serrano 119, 28006 Madrid, Spain.
Aurora NogalesInstituto de Estructura de la Materia, IEM-CSIC, Serrano 121, 28006 Madrid, Spain.ORCID https://orcid.org/0000-0002-2494-3551
Mari Cruz García-GutiérrezInstituto de Estructura de la Materia, IEM-CSIC, Serrano 121, 28006 Madrid, Spain.ORCID https://orcid.org/0000-0002-3604-1512
Gonzalo SantoroInstituto de Estructura de la Materia, IEM-CSIC, Serrano 121, 28006 Madrid, Spain.ORCID https://orcid.org/0000-0003-4751-2209
Izabela IrskaDepartment of Mechanical Engineering and Mechatronics, West Pomeranian University of Technology, Al. Piastów 19, PL 70310 Szczecin, Poland.ORCID https://orcid.org/0000-0002-5521-1847
Sandra PaszkiewiczDepartment of Mechanical Engineering and Mechatronics, West Pomeranian University of Technology, Al. Piastów 19, PL 70310 Szczecin, Poland.
Anna SzymczykDepartment of Mechanical Engineering and Mechatronics, West Pomeranian University of Technology, Al. Piastów 19, PL 70310 Szczecin, Poland.ORCID https://orcid.org/0000-0002-9670-6395
Tiberio A EzquerraInstituto de Estructura de la Materia, IEM-CSIC, Serrano 121, 28006 Madrid, Spain.ORCID https://orcid.org/0000-0001-9966-519X

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Here, we present a detailed description of the in situ isothermal crystallization of poly(trimethylene 2,5-furandicarboxylate)(PTF) as revealed by real-time Fourier transform infrared spectroscopy (FTIR) and grazing incidence wide-angle X-ray scattering (GIWAXS). From FTIR experiments, the evolution of hydrogen bonding with crystallization time can be monitored in real time, while from GIWAXS, crystal formation can be followed. Density functional theory (DFT) calculations have been used to simulate FTIR spectra for different theoretical structures, enabling a precise band assignment. In addition, based on DFT

Identifiers

PMID38495385
PMCPMC10938886

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.