ArticleNanomaterials (Basel, Switzerland)2024
Effect of Synthesis Conditions on CuO-NiO Nanocomposites Synthesized via Saponin-Green/Microwave Assisted-Hydrothermal Method.
Article in Nanomaterials (Basel, Switzerland), 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 5 papers.
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Who cites it
5 citing papers in PubMed.
- Influence of cobalt/manganese ratio on structural, magnetic, and antibacterial properties of spinel ferrite nanocomposites synthesized by novel henna-green/microwave-assisted hydrothermal method.Scientific reports · 2026Article
- Magnetic and antibacterial properties of substituted cobalt spinel ferrite nanocomposites synthesized via henna green microwave hydrothermal method.Scientific reports · 2025Article
- Plant extract-mediated green-synthesized CuO nanoparticles for environmental and microbial remediation: a review covering basic understandings to mechanistic study.Nanoscale advances · 2025Review
- The Effect of Composition on the Properties and Application of CuO-NiO Nanocomposites Synthesized Using a Saponin-Green/Microwave-Assisted Hydrothermal Method.International journal of molecular sciences · 2024Article
- Photocatalytic Degradation of Organic Pollutants-Nile Blue, Methylene Blue, and Bentazon Herbicide-Using NiO-ZnO Nanocomposite.Nanomaterials (Basel, Switzerland) · 2024Article
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Authors and funding
7 authors.
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Abstract
This work presents the synthesis of CuO-NiO nanocomposites under different synthesis conditions. Nanocomposites were synthesized by merging a green synthesis process with a microwave-assisted hydrothermal method. The synthesis conditions were as follows: concentration of the metal precursors (0.05, 0.1, and 0.2 M), pH (9, 10, and 11), synthesis temperature (150 °C, 200 °C, and 250 °C), microwave treatment time (15, 30, and 45 min), and extract concentration (20 and 40 mL of 1 g saponin/10 mL water, and 30 mL of 2 g saponin/10 mL water). The phases and crystallite sizes of the calcined nanocomposites were characterized using XRD and band gap via UV-Vis spectroscopy, and their morphologies were investigated using SEM and TEM. The XRD results confirmed the formation of a face-centered cubic phase for nickel oxide, while copper oxide has a monoclinic phase. The calculated crystallite size was in the range of 29-39 nm. The direct band gaps of the samples prepared in this work were in the range of 2.39-3.17 eV.
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