ArticleScience advances2024
Selective formation of metastable polymorphs in solid-state synthesis.
Article in Science advances, 2024. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 8 papers.
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Who cites it
8 citing papers in PubMed.
- Machine Learning-Driven Nanoscale Synthesis for Electrocatalytic Performance: From Data-Driven Methodologies to Closed-Loop Optimization.Advanced materials (Deerfield Beach, Fla.) · 2026Review
- Programming stacking order in conducting van der Waals metal-organic frameworks through ligand aggregation.Nature chemistry · 2026Article
- Metastable Nickel Carbide Enables Programmable Evolution of Nanoporous Carbon Architectures.Small (Weinheim an der Bergstrasse, Germany) · 2026Article
- Amorphous intermediates and discovery of a kinetic polymorph of BiVONature communications · 2026Article
- Process Development for the Continuous Manufacturing of Carbamazepine-Nicotinamide Co-Crystals Utilizing Hot-Melt Extrusion Technology.Pharmaceutics · 2025Article
- How to accelerate the inorganic materials synthesis: from computational guidelines to data-driven method?National science review · 2025Review
- Quantifying the regime of thermodynamic control for solid-state reactions during ternary metal oxide synthesis.Science advances · 2024Article
- Autonomous and dynamic precursor selection for solid-state materials synthesis.Nature communications · 2023Article
Corrections and comments
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Authors and funding
9 authors.
Funding
No grant is acknowledged in the PubMed record.
Abstract
Metastable polymorphs often result from the interplay between thermodynamics and kinetics. Despite advances in predictive synthesis for solution-based techniques, there remains a lack of methods to design solid-state reactions targeting metastable materials. Here, we introduce a theoretical framework to predict and control polymorph selectivity in solid-state reactions. This framework presents reaction energy as a rarely used handle for polymorph selection, which influences the role of surface energy in promoting the nucleation of metastable phases. Through in situ characterization and density functional theory calculations on two distinct synthesis pathways targeting LiTiOPO
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Registered trials
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