Evidence map›Paper›PMID 38069405›Full record

ArticleInternational journal of molecular sciences2023

Synthesis of Novel Phosphorus-Containing Derivatives of 1,3,4-Trimethylglycoluril via the Birum-Oleksyszyn Reaction.

Sergey I Gorbin, Abdigali A Bakibaev, Vera P Tuguldurova, Andrey V Kotov, Gleb O Sysoev, Andrei S Potapov, Dmitry I Pavlov, Victor S Malkov, Alexey S Knyazev, Dmitriy A Kurgachev and 1 more

Open access · goldAbstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in International journal of molecular sciences, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

0numbers the graph read from it
0cells of the map it votes in
0citing papers in PubMed
0.1field-weighted citation impact, top 52% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed, 1 citations in OpenAlex.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

11 authors at 2 institutions in 1 country.

Sergey I GorbinDepartment of Chemistry, Tomsk State University, 36, Lenin Avenue, Tomsk 634050, Russia.
Abdigali A BakibaevDepartment of Chemistry, Tomsk State University, 36, Lenin Avenue, Tomsk 634050, Russia.
Vera P TuguldurovaDepartment of Chemistry, Tomsk State University, 36, Lenin Avenue, Tomsk 634050, Russia.ORCID 0000-0002-1015-1123
Andrey V KotovDepartment of Chemistry, Tomsk State University, 36, Lenin Avenue, Tomsk 634050, Russia.ORCID 0009-0009-6623-7522
Gleb O SysoevDepartment of Chemistry, Tomsk State University, 36, Lenin Avenue, Tomsk 634050, Russia.
Andrei S PotapovNikolaev Institute of Inorganic Chemistry, 3 Lavrentiev Avenue, Novosibirsk 630090, Russia.ORCID 0000-0003-2360-7473
Dmitry I PavlovNikolaev Institute of Inorganic Chemistry, 3 Lavrentiev Avenue, Novosibirsk 630090, Russia.ORCID 0000-0002-5996-8062
Victor S MalkovDepartment of Chemistry, Tomsk State University, 36, Lenin Avenue, Tomsk 634050, Russia.ORCID 0000-0003-4532-2882
Alexey S KnyazevDepartment of Chemistry, Tomsk State University, 36, Lenin Avenue, Tomsk 634050, Russia.
Dmitriy A KurgachevDepartment of Chemistry, Tomsk State University, 36, Lenin Avenue, Tomsk 634050, Russia.
Mark V MichalchenkovDepartment of Chemistry, Tomsk State University, 36, Lenin Avenue, Tomsk 634050, Russia.
National Research Tomsk State University · RUNikolaev Institute of Inorganic Chemistry · RU

Funding

National Research Tomsk State University Tomsk State University Development Programme (Priority 2030)
6 · The paper itself

Abstract

This work presents the synthesis of a new compound, 1-[aryl-(diphenylphosphono)methyl]-3,4,6-trimethylglycolurils, via the interaction of benzaldehyde and its mononitro- and monohydroxyderivatives with 1,3,4-trimethylglycoluril and triphenylphosphite. By varying the reaction conditions and the catalysts, the obtained product yields ranged from satisfactory to good. The diastereomers formed during the reaction were separated by semipreparative HPLC on the C18 stationary phase. The isolated diastereomers were characterized by

Indexed as

1,3,4-trimethylglycolurilaryldiphenylphosphonatesBirum–Oleksyszyn reactiondiastereomers

Identifiers

PMID38069405
PMCPMC10707106
OpenAlexW4389286197

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.