Evidence map›Paper›PMID 37968362›Full record

ArticleScientific reports2023

Green and sustainable synthesis of CaO nanoparticles: Its solicitation as a sensor material and electrochemical detection of urea.

T S Sunil Kumar Naik, Simranjeet Singh, Pavithra Narasimhappa, Radhika Varshney, Joginder Singh, Nadeem A Khan, Sasan Zahmatkesh, Praveen C Ramamurthy, Nabila Shehata, G N Kiran and 1 more

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Article in Scientific reports, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 4 papers.

0numbers the graph read from it
0cells of the map it votes in
4citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

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Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

4 citing papers in PubMed.

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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

11 authors.

T S Sunil Kumar NaikDepartment of Materials Engineering, Indian Institute of Science, Bangalore, 560012, India.
Simranjeet Singh *Interdisciplinary Centre for Water Research (ICWaR), Indian Institute of Science, Bangalore, 560012, India.
Pavithra NarasimhappaInterdisciplinary Centre for Water Research (ICWaR), Indian Institute of Science, Bangalore, 560012, India.
Radhika VarshneyInterdisciplinary Centre for Water Research (ICWaR), Indian Institute of Science, Bangalore, 560012, India.
Joginder SinghDepartment of Botany, Nagaland University, Lumami, Nagaland, 798627, India.
Nadeem A Khan *Interdisciplinary Research Center for Membranes and Water Security (IRC-MWS), King Fahd University of Petroleum and Minerals, Dhahran, 31261, Saudi Arabia. nadeem.khan@kfupm.edu.sa.
Sasan ZahmatkeshTecnologico de Monterrey, Escuela de Ingenieríay Ciencias, Puebla, Mexico.
Praveen C RamamurthyDepartment of Materials Engineering, Indian Institute of Science, Bangalore, 560012, India. onegroupb203@gmail.com.
Nabila ShehataEnvironmental Science and Industrial Development Department, Faculty of Postgraduate Studies for Advanced Sciences, Beni-Suef University, Beni-Suef, Egypt.
G N KiranDepartment of Chemistry, SSIT, Sri Siddhartha Academy of Higher Education, Tumkur, Karnataka, 572107, India.
K SunilDepartment of Chemistry, SSIT, Sri Siddhartha Academy of Higher Education, Tumkur, Karnataka, 572107, India.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Urea is recognized as one of the most frequently used adulterants in milk to enhance artificial protein content, and whiteness. Drinking milk having high urea concentrations which causes innumerable health disputes like ulcers, indigestion, and kidney-related problems. Therefore, herein, a simple and rapid electroanalytical platform was developed to detect the presence of urea in milk using a modified electrode sensor. Calcium oxide nanoparticles (CaO NPs) were green synthesized and used as a catalyst material for developing the sensor. Synthesized materials formation was confirmed by different techniques like FTIR, UV-visible, XRD, SEM-EDX, and Raman spectroscopy. The carbon paste electrode (CPE) was modified using the CaO NPs and used as a working electrode during the analysis followed by cyclic voltammetry and differential pulse voltammetry (DPV) techniques. The fabricated calcium oxide modified carbon paste electrode (CaO/CPE) successfully detected the presence of urea in the lower concentration range (lower limit of detection (LLOD) = 0.032 µM) having a wide linear detection range of 10-150 µM. Adsorption-controlled electrode process was achieved at the scan rate variation parameter. The leading parameters like the selectivity, repeatability, and stability of the CaO/CPE were investigated. The relative standard deviation of sensor was ± 3.8% during the interference and stability study.

Identifiers

PMID37968362
PMCPMC10651922

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