ArticleMagnetic resonance (Gottingen, Germany)2021
A cryogen-free, semi-automated apparatus for bullet-dynamic nuclear polarization with improved resolution.
Article in Magnetic resonance (Gottingen, Germany), 2021. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 15 papers.
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Who cites it
15 citing papers in PubMed.
- Proton signal enhancement of three orders of magnitude in high-field liquid-state NMR.Nature communications · 2026Article
- Signal averaging in cryogenic fast-field-cycling NMR experiments.Scientific reports · 2026Article
- Single-scan detection of ligand-binding using hyperpolarization and low-field relaxation.Communications chemistry · 2026Article
- Chemically induced deceleration of nuclear spin relaxation (CIDER) preserves hyperpolarization.Science advances · 2025Article
- Cryogenic sample eject system for electron paramagnetic resonance spectrometers.Journal of magnetic resonance (San Diego, Calif. : 1997) · 2025Article
- Bullet-DNP Enables NMR Spectroscopy of Pyruvate and Amino Acids at Nanomolar to Low Micromolar Concentrations.Analytical chemistry · 2024Article
- Short-lived calcium carbonate precursors observed in situ via Bullet-dynamic nuclear polarization.Communications chemistry · 2024Article
- Hyperpolarization of Long-Lived States of Protons in Aliphatic Chains by Bullet Dynamic Nuclear Polarization, Revealed on the Fly by Spin-Lock-Induced Crossing.The journal of physical chemistry letters · 2024Article
- Long-lived enhanced magnetization-A practical metabolic MRI contrast material.Science advances · 2024Article
- Spin Hyperpolarization in Modern Magnetic Resonance.Chemical reviews · 2023Review
- Primary Structure of Glycans by NMR Spectroscopy.Chemical reviews · 2023Review
- Introduction to "Geoffrey Bodenhausen Festschrift".Magnetic resonance (Gottingen, Germany) · 2023Article
- Radical-Induced Low-FieldThe journal of physical chemistry letters · 2022Article
- Toward protein NMR at physiological concentrations by hyperpolarized water-Finding and mapping uncharted conformational spaces.Science advances · 2022Article
- Fine optimization of a dissolution dynamic nuclear polarization experimental setting forMagnetic resonance (Gottingen, Germany) · 2022Article
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Authors and funding
5 authors.
Funding
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Abstract
In dissolution-dynamic nuclear polarization, a hyperpolarized solid is dissolved with a jet of hot solvent. The solution is then transferred to a secondary magnet, where spectra can be recorded with improved sensitivity. In bullet-dynamic nuclear polarization this order is reversed. Pressurized gas is used to rapidly transfer the hyperpolarized solid to the secondary magnet, and the hyperpolarized solid is dissolved only upon arrival. A potential advantage of this approach is that it may avoid excessive dilution and the associated signal loss, in particular for small sample quantities. Previously, we have shown that liquid-state NMR spectra with polarization levels of up to 30 % may be recorded within less than 1 s after the departure of the hyperpolarized solid from the polarizing magnet. The resolution of the recorded spectra however was limited. The system consumed significant amounts of liquid helium, and substantial manual work was required in between experiments to prepare for the next shot. Here, we present a new bullet-DNP (dynamic nuclear polarization) system that addresses these limitations.
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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.