Evidence map›Paper›PMID 37896341›Full record

ArticlePolymers2023

Composite Polymer Granules Based on Poly-ε-Caprolactone and Montmorillonite Prepared by Solution-Casting and Melt Extrusion.

Anna Sukhanova, Anatoly Boyandin, Natalya Ertiletskaya, Taisia Shalygina, Alexander Shabanov, Alexander Vasiliev, Ivan Obvertkin, Valeria Brott, Yulia Prokopchuk, Alexander Samoilo

Open access · goldAbstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Polymers, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
0.7field-weighted citation impact, top 36% of its field
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed, 7 citations in OpenAlex.

  1. Review
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

10 authors at 3 institutions in 1 country.

Anna SukhanovaDepartment of Biodegradable Polymers Materials, Reshetnev Siberian State University of Science and Technology, 31 Krasnoyarskiy Rabochiy Av., Krasnoyarsk 660037, Russia.
Anatoly BoyandinDepartment of Biodegradable Polymers Materials, Reshetnev Siberian State University of Science and Technology, 31 Krasnoyarskiy Rabochiy Av., Krasnoyarsk 660037, Russia.ORCID 0000-0002-9190-2792
Natalya ErtiletskayaDepartment of Biodegradable Polymers Materials, Reshetnev Siberian State University of Science and Technology, 31 Krasnoyarskiy Rabochiy Av., Krasnoyarsk 660037, Russia.ORCID 0000-0003-2626-893X
Taisia ShalyginaDepartment of Analysis, Synthesis, Modeling and Digital Design of Smart Materials with Specified Properties, Reshetnev Siberian State University of Science and Technology, 31 Krasnoyarskiy Rabochiy Av., Krasnoyarsk 660037, Russia.ORCID 0000-0002-1720-1867
Alexander ShabanovDepartment of Molecular Spectroscopy, Kirensky Institute of Physics, Federal Research Center "Krasnoyarsk Science Center SB RAS", 50/38 Akademgorodok, Krasnoyarsk 660036, Russia.ORCID 0000-0002-2389-4698
Alexander VasilievDepartment Engineering Physics and Radio Electronics, Siberian Federal University, 79 Svobodny Av., Krasnoyarsk 660041, Russia.
Ivan ObvertkinDepartment of Digital Design of Transformable Structures based on Smart Materials, Reshetnev Siberian State University of Science and Technology, 31 Krasnoyarskiy Rabochiy Av., Krasnoyarsk 660037, Russia.
Valeria BrottDepartment of Biodegradable Polymers Materials, Reshetnev Siberian State University of Science and Technology, 31 Krasnoyarskiy Rabochiy Av., Krasnoyarsk 660037, Russia.
Yulia ProkopchukDepartment of Biodegradable Polymers Materials, Reshetnev Siberian State University of Science and Technology, 31 Krasnoyarskiy Rabochiy Av., Krasnoyarsk 660037, Russia.
Alexander SamoiloDepartment of Biodegradable Polymers Materials, Reshetnev Siberian State University of Science and Technology, 31 Krasnoyarskiy Rabochiy Av., Krasnoyarsk 660037, Russia.
Siberian State Aerospace University · RUSiberian Federal University · RUInstitute of Physics · RU

Funding

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6 · The paper itself

Abstract

Eco-friendly polymer composites in the form of granules based on biodegradable polycaprolactone (PCL) with the inclusion of montmorillonite (MMT) from 5 to 50 wt% were prepared by solution-casting and melt extrusion. The physicochemical properties of the composite granules were studied using FTIR spectroscopy, XRDA, DSC, and TGA methods. The paper presents comparative values of crystallinity of composite granules which depend on the method of measuring (XRDA, DSC). It was shown that the crystallinity of PCL/MMT granules was affected by the preparation method and by the MMT content, and that with increase in MMT content, crystallinity increased by up to 61-67%. The change in crystallinity of the granules also affected its biodegradation in soil. At the end of exposure in soil, the mass loss for the granules prepared by solution-casting was more than 90%, whereas for the composite granules prepared by extrusion it was less than 60%. Applying melt extrusion enabled obtaining intercalated composites with predictable features, whereas only mixed-structure microcomposites could be prepared by solution-casting.

Indexed as

biodegradable polymersmontmorillonitepolymer compositespoly-ε-caprolactoneprocessing technologies

Identifiers

PMID37896341
PMCPMC10610963
OpenAlexW4387671386

What OpenQuestion holds

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LicenceCC BY
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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.