Evidence map›Paper›PMID 37786855›Full record

ArticleJournal of veterinary research2023

Inter-laboratory validation of liquid chromatography-tandem mass spectrometry multi-mycotoxin determination in animal feed - method transfer from the reference laboratory to regional laboratories.

Piotr Jedziniak, Łukasz Panasiuk, Katarzyna Pietruszka, Krzysztof Kolano, Radosław Zbytniewski

Abstract read
In one paragraph

Article in Journal of veterinary research, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

5 authors.

Piotr JedziniakDepartment of Pharmacology and Toxicology, National Veterinary Research Institute, 24-100 Puławy, Poland.
Łukasz PanasiukDepartment of Pharmacology and Toxicology, National Veterinary Research Institute, 24-100 Puławy, Poland.
Katarzyna PietruszkaDepartment of Pharmacology and Toxicology, National Veterinary Research Institute, 24-100 Puławy, Poland.
Krzysztof KolanoDepartment of Veterinary Hygiene, Provincial Veterinary Inspectorate, 30-965 Kraków, Poland.
Radosław ZbytniewskiDepartment of Veterinary Hygiene, Provincial Veterinary Inspectorate, 85-090 Bydgoszcz, Poland.

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

Introduction: The results are presented of the inter-laboratory validation of a liquid chromatography-tandem mass spectrometry method for the determination of eight mycotoxins (aflatoxin B1, deoxynivalenol, fumonisin B1, fumonisin B2, ochratoxin A, toxin T-2, toxin HT-2 and zearalenone) in animal feeds. Material and Methods: This study was an essential part of the method's transfer from the National Reference Laboratory to six regional laboratories in Poland working in the official survey of mycotoxins in feed. The laboratories received a batch of standard solutions, blank samples and quality control materials on which to perform analysis with one procedure and different liquid chromatography-tandem mass spectrometry conditions. Results: The validation results show good precision (reproducibility coefficient of variation 3.7-20.5%) and accuracy of the method (recovery 89-120% and trueness 94-103%) and sufficient skills of the laboratory personnel. Conclusion: The study is an example of the successful transfer of the method among laboratories.

Indexed as

feedinter-laboratory comparisonmass spectrometrymycotoxinsvalidation

Identifiers

PMID37786855
PMCPMC10541672

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Registered trials

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.