ArticlePolymers2023
Investigation of Curing Process and Thermal Behavior of Copolymers Based on Polypropylene Glycol Fumarate and Acrylic Acid Using the Methods of DSC and TGA.
Article in Polymers, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.
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The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.
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Who cites it
3 citing papers in PubMed, 5 citations in OpenAlex.
- Thermosetting Resins Based on Poly(Ethylene Glycol Fumarate) and Acrylic Acid: Rheological and Thermal Analysis.Molecules (Basel, Switzerland) · 2025Article
- Influence of Mineral Fillers on the Curing Process and Thermal Degradation of Polyethylene Glycol Maleate-Acrylic Acid-Based Systems.Polymers · 2025Article
- Poly(propylene fumarate)/hydroxyapatite nanocomposite/black phosphorus nanosheet phosphate composites for enhanced bone repair.Journal of orthopaedic surgery and research · 2025Article
Corrections and comments
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Authors and funding
5 authors at 1 institution in 1 country.
Funding
Abstract
In this work, the possibility of preparation of copolymers of three-dimensional crosslinked structure based on polypropylene glycol fumarate and acrylic acid is shown. The initial reagent polypropylene glycol fumarate has been synthesized by polycondensation reaction of fumaric acid and propylene glycol. The curing process of polypropylene glycol fumarate and acrylic acid at various mole concentrations was studied using DSC method at isothermal and dynamic regimens. Curing in isothermal condition was carried out at temperatures of 60 °C, 70 °C, and 80 °C. Residual reactivity was evaluated at a dynamic regimen within the temperature range from 30 °C to 200 °C at a constant heating rate. On the basis of calorimetric studies, the thermal effects and kinetic parameters of the reaction (conversion, reaction rate, activation energy) have been determined. Thermal behavior of cured samples of p-PGF-AA was estimated using dynamic thermogravimetry (TGA). According to TGA data, the process of decomposition of the studied copolymers proceeds in several stages. Based on the results obtained, the activation energies of thermal decomposition were calculated using the iso-conversional methods of Kissinger-Akakhira-Sunose and Friedman.
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Registered trials
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