ArticleNanomaterials (Basel, Switzerland)2023
Exploring Pt-Pd Alloy Nanoparticle Cluster Formation through Conventional Sizing Techniques and Single-Particle Inductively Coupled Plasma-Sector Field Mass Spectrometry.
Article in Nanomaterials (Basel, Switzerland), 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.
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3 citing papers in PubMed.
- An Unprecedented Metal Distribution in Silica Nanoparticles Determined by Single-Particle Inductively Coupled Plasma Mass Spectrometry.Nanomaterials (Basel, Switzerland) · 2024Article
- ICP-MS-Based Characterization and Quantification of Nano- and Microstructures.Nanomaterials (Basel, Switzerland) · 2024Article
- Synthesis and Unique Behaviors of High-Purity HEA Nanoparticles Using Femtosecond Laser Ablation.Nanomaterials (Basel, Switzerland) · 2024Article
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8 authors.
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Abstract
Accurate characterization of Pt-Pd alloy nanoparticle clusters (NCs) is crucial for understanding their synthesis using Gas-Diffusion Electrocrystallization (GDEx). In this study, we propose a comprehensive approach that integrates conventional sizing techniques-scanning electron microscopy (SEM) and dynamic light scattering (DLS)-with innovative single-particle inductively coupled plasma-sector field mass spectrometry (spICP-SFMS) to investigate Pt-Pd alloy NC formation. SEM and DLS provide insights into morphology and hydrodynamic sizes, while spICP-SFMS elucidates the particle size and distribution of Pt-Pd alloy NCs, offering rapid and orthogonal characterization. The spICP-SFMS approach presented enables detailed characterization of Pt-Pd alloy NCs, which was previously challenging due to the absence of multi-element capabilities in conventional spICP-MS systems. This innovative approach not only enhances our understanding of bimetallic nanoparticle synthesis, but also paves the way for tailoring these materials for specific applications, marking a significant advancement in the field of nanomaterial science.
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