Evidence map›Paper›PMID 37594864›Full record

ArticleJournal of synchrotron radiation2023

Development of a versatile electrochemical cell for in situ grazing-incidence X-ray diffraction during non-aqueous electrochemical nitrogen reduction.

Sarah J Blair, Adam C Nielander, Kevin H Stone, Melissa E Kreider, Valerie A Niemann, Peter Benedek, Eric J McShane, Alessandro Gallo, Thomas F Jaramillo

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Journal of synchrotron radiation, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 2 papers.

0numbers the graph read from it
0cells of the map it votes in
2citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

2 citing papers in PubMed.

  1. Probing Buried Interfaces in Batteries: TowardChemistry of materials : a publication of the American Chemical Society · 2026
    Review
  2. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

9 authors.

Sarah J BlairChemical Engineering, Stanford University, 443 Via Ortega, Stanford, CA 94305, USA.ORCID 0000-0001-6680-0199
Adam C NielanderSUNCAT Center for Interface Science and Catalysis, SLAC National Accelerator Laboratory, 2575 Sand Hill Rd, Menlo Park, CA 94025, USA.ORCID 0000-0002-3639-2427
Kevin H StoneStanford Synchrotron Radiation Lightsource, SLAC National Accelerator Laboratory, 2575 Sand Hill Rd, Menlo Park, CA 94025, USA.ORCID 0000-0003-1387-1510
Melissa E KreiderChemical Engineering, Stanford University, 443 Via Ortega, Stanford, CA 94305, USA.ORCID 0000-0003-1750-6860
Valerie A NiemannChemical Engineering, Stanford University, 443 Via Ortega, Stanford, CA 94305, USA.ORCID 0000-0002-9565-022X
Peter BenedekChemical Engineering, Stanford University, 443 Via Ortega, Stanford, CA 94305, USA.ORCID 0000-0001-8560-2278
Eric J McShaneChemical Engineering, Stanford University, 443 Via Ortega, Stanford, CA 94305, USA.ORCID 0000-0002-2456-8798
Alessandro GalloSUNCAT Center for Interface Science and Catalysis, SLAC National Accelerator Laboratory, 2575 Sand Hill Rd, Menlo Park, CA 94025, USA.ORCID 0000-0003-4687-8188
Thomas F JaramilloChemical Engineering, Stanford University, 443 Via Ortega, Stanford, CA 94305, USA.ORCID 0000-0001-9900-0622

Funding

US Department of Energy, Office of Science DE-AC02-76SF00515Villum Fonden 9455
6 · The paper itself

Abstract

In situ techniques are essential to understanding the behavior of electrocatalysts under operating conditions. When employed, in situ synchrotron grazing-incidence X-ray diffraction (GI-XRD) can provide time-resolved structural information of materials formed at the electrode surface. In situ cells, however, often require epoxy resins to secure electrodes, do not enable electrolyte flow, or exhibit limited chemical compatibility, hindering the study of non-aqueous electrochemical systems. Here, a versatile electrochemical cell for air-free in situ synchrotron GI-XRD during non-aqueous Li-mediated electrochemical N

Indexed as

electrocatalysiselectrochemical cell designgrazing incidencein situnon-aqueous Li-mediated electrochemical nitrogen reductionsolid electrolyte interphasesynchrotron X-ray diffraction

Identifiers

PMID37594864
PMCPMC10481268

What OpenQuestion holds

Textmetadata
LicenceCC BY
Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.