Evidence map›Paper›PMID 37555210›Full record

ArticleJournal of applied crystallography2023

Towards scanning nanostructure X-ray microscopy.

Anton Kovyakh, Soham Banerjee, Chia-Hao Liu, Christopher J Wright, Yuguang C Li, Thomas E Mallouk, Robert Feidenhans'l, Simon J L Billinge

Abstract read
PubMed Full text at PMC Publisher
In one paragraph

Article in Journal of applied crystallography, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 1 paper.

0numbers the graph read from it
0cells of the map it votes in
1citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

1 citing paper in PubMed.

  1. Article
4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

8 authors.

Anton KovyakhNiels Bohr Institute, University of Copenhagen, Universitetsparken 5, DK-2100 Copenhagen, Denmark.ORCID https://orcid.org/0000-0002-2165-6354
Soham BanerjeeDepartment of Applied Physics and Applied Mathematics, Columbia University, New York, NY 10027, USA.
Chia-Hao LiuDepartment of Applied Physics and Applied Mathematics, Columbia University, New York, NY 10027, USA.ORCID https://orcid.org/0000-0002-3216-0354
Christopher J WrightDepartment of Applied Physics and Applied Mathematics, Columbia University, New York, NY 10027, USA.ORCID https://orcid.org/0000-0003-2522-7028
Yuguang C LiDepartment of Chemistry, University at Buffalo, The State University of New York, Buffalo, New York, NY 14260, USA.
Thomas E MalloukDepartment of Chemistry, The University of Pennsylvania, Philadelphia, PA, USA.
Robert Feidenhans'lNiels Bohr Institute, University of Copenhagen, Universitetsparken 5, DK-2100 Copenhagen, Denmark.
Simon J L BillingeDepartment of Applied Physics and Applied Mathematics, Columbia University, New York, NY 10027, USA.ORCID https://orcid.org/0000-0002-9734-4998

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

This article demonstrates spatial mapping of the local and nanoscale structure of thin film objects using spatially resolved pair distribution function (PDF) analysis of synchrotron X-ray diffraction data. This is exemplified in a lab-on-chip combinatorial array of sample spots containing catalytically interesting nanoparticles deposited from liquid precursors using an ink-jet liquid-handling system. A software implementation is presented of the whole protocol, including an approach for automated data acquisition and analysis using the atomic PDF method. The protocol software can handle semi-automated data reduction, normalization and modeling, with user-defined recipes generating a comprehensive collection of metadata and analysis results. By slicing the collection using included functions, it is possible to build images of different contrast features chosen by the user, giving insights into different aspects of the local structure.

Indexed as

atomic pair distribution functionnanoparticlesspatial mappingthin films

Identifiers

PMID37555210
PMCPMC10405596

What OpenQuestion holds

Textmetadata
LicenceCC BY
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Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.