Evidence map›Paper›PMID 37458876›Full record

ArticleMikrochimica acta2023

Synthesis of a novel magnetic nanomaterial for the development of a multielemental speciation method of lead, mercury, and vanadium via HPLC-ICP MS.

Pablo Montoro-Leal, Juan Carlos García-Mesa, Irene Morales-Benítez, Laura Vázquez-Palomo, María Del Mar López Guerrero, Elisa I Vereda Alonso

Abstract read
In one paragraph

Article in Mikrochimica acta, 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Cited by 3 papers.

0numbers the graph read from it
0cells of the map it votes in
3citing papers in PubMed
–field-weighted citation impact
1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

3 citing papers in PubMed.

  1. Article
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4 · The record

Corrections and comments

PubMed lists nothing against this paper. Absence here is not a guarantee, only a check that was made.

5 · Who and what money

Authors and funding

6 authors.

Pablo Montoro-Leal *Department of Analytical Chemistry, Faculty of Sciences, University of Malaga, 29071, Málaga, Spain.
Juan Carlos García-Mesa *Department of Analytical Chemistry, Faculty of Sciences, University of Malaga, 29071, Málaga, Spain.
Irene Morales-Benítez *Department of Analytical Chemistry, Faculty of Sciences, University of Malaga, 29071, Málaga, Spain.
Laura Vázquez-PalomoDepartment of Analytical Chemistry, Faculty of Sciences, University of Malaga, 29071, Málaga, Spain.
María Del Mar López GuerreroDepartment of Analytical Chemistry, Faculty of Sciences, University of Malaga, 29071, Málaga, Spain.
Elisa I Vereda AlonsoDepartment of Analytical Chemistry, Faculty of Sciences, University of Malaga, 29071, Málaga, Spain. eivereda@uma.es.ORCID http://orcid.org/0000-0001-9502-4424

Funding

No grant is acknowledged in the PubMed record.

6 · The paper itself

Abstract

A new magnetic functionalized material based on graphene oxide magnetic nanoparticles named by us, M@GO-TS, was designed and characterized in order to develop a magnetic solid-phase extraction method (MSPE) to enrich inorganic and organic species of lead, mercury, and vanadium. A flow injection (FI) system was used to preconcentrate the metallic and organometallic species simultaneously, while the ultra-trace separation and determination of the selected species were achieved by high-performance liquid chromatography coupled to inductively coupled plasma mass spectrometry (HPLC-ICP MS). Therefore, preconcentration and separation/determination processes were automated and conducted separately. To the best of our knowledge, this is the first method combining an online MSPE and HPLC-ICP MS for multielemental speciation. Under the optimized conditions, the enrichment factor obtained for Pb

Indexed as

HPLC-ICP MSMagnetic graphene oxideMultielemental speciationSolid-phase extraction

Identifiers

PMID37458876
PMCPMC10352391

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Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.