Applicability and Limitations of a Capillary-LC Column-Switching System Using Hybrid Graphene-Based Stationary Phases.

João Victor Basolli Borsatto, Edvaldo Vasconcelos Soares Maciel, Alejandro Cifuentes, Fernando Mauro Lanças

Open access · goldAbstract read

In one paragraph

Article in Molecules (Basel, Switzerland), 2023. The graph could read no effect estimate from its abstract, so it casts no vote on the map. Not yet cited in PubMed.

0numbers the graph read from it

0cells of the map it votes in

0citing papers in PubMed

0.1field-weighted citation impact, top 60% of its field

1 · What the graph read from it

What it found

Each row is one number read from the abstract, on the scale the paper reported it, with its interval. Left of the dashed line favours the treatment, right favours the comparator. Under each row is the sentence it came from. New to these charts? A ten-minute tutorial.

The abstract states no effect estimate the extractor could read, or names no intervention and outcome on the map, so this paper lights no cell and moves no belief. It is still indexed, cited and linked below.

2 · The registry

The trial behind it

Trials whose registry record cites this paper, or whose number appears in the abstract. A trial that started after this paper was published is citing it as background, not reporting it.

Neither the registry nor the abstract names a trial number. If this is a trial report, that itself is worth knowing.

3 · Its place in the literature

Who cites it

0 citing papers in PubMed, 1 citations in OpenAlex.

No citing paper in PubMed yet.

4 · The record

Corrections and comments

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5 · Who and what money

Authors and funding

4 authors at 2 institutions in 3 countries.

João Victor Basolli BorsattoLaboratory of Chromatography, Institute of Chemistry at Sao Carlos, University of Sao Paulo, P.O. Box 780, Sao Carlos 13566590, Brazil.ORCID 0000-0002-1890-6076

Edvaldo Vasconcelos Soares MacielLaboratory of Chromatography, Institute of Chemistry at Sao Carlos, University of Sao Paulo, P.O. Box 780, Sao Carlos 13566590, Brazil.ORCID 0000-0002-1231-7190

Alejandro CifuentesLaboratory of Foodomics, Institute of Food Science Research (CIAL, CSIC), Nicolás Cabrera 9, 28049 Madrid, Spain.ORCID 0000-0002-7464-0217

Fernando Mauro LançasLaboratory of Chromatography, Institute of Chemistry at Sao Carlos, University of Sao Paulo, P.O. Box 780, Sao Carlos 13566590, Brazil.

Universidade de São Paulo · BRInstituto de Investigación en Ciencias de la Alimentación · ES

Funding

CAPES Finance Code 001CNPq 307293/2014-9; 308843/ 2019-3; Proc. 142513/2019-9São Paulo Research Foundation 2019/22724-7, 2017/02147-0Spanish Ministry of Science and Innovation PID2020-113050RB-I00 project

6 · The paper itself

Abstract

Graphene oxide sheets fixed over silica particles (SiGO) and their modification functionalized with C18 and endcapped (SiGO-C18ec) have been reported as sorbents for extraction and analytical columns in LC. In this study, a SiGO column was selected as the extraction column and a SiGO-C18ec as the analytical column to study the applicability and limitations of a column-switching system composed exclusively of columns packed with graphene-based sorbents. Pyriproxyfen and abamectin B1a were selected as the analytes, and orange-flavored carbonated soft drinks as the matrix. The proposed system could be successfully applied to the pyriproxyfen analysis in a concentration range between 0.5 to 25 µg/mL presenting a linearity of R

Indexed as

GraphiteIvermectinSilicon DioxideabamectinGraphiteIvermectinSilicon Dioxidecapillary liquid chromatographycolumn switchingdirect injectiongraphene-based materialspacked columnSiGOSiGO-C18ec

Identifiers

PMID37446660

DOI10.3390/molecules28134999

PMCPMC10343772

OpenAlexW4382466067

What OpenQuestion holds

Textmetadata

LicenceCC BY

Read underepoch 390

Registered trials

None linked

Read under generation 80e0d062 · epoch 390. Bibliography from PubMed, PubMed Central and OpenAlex; grants from NIH RePORTER; trial links from ClinicalTrials.gov; estimates, votes and beliefs from the OpenQuestion graph.